GCMS analysis results for sample AE08065, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08065 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046771–000046785

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08065.D Vial: 22 Acq On : 16 Apr 2002 3:59 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.28 ug/L 380875 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-dlO 188 C14D10 001517-22-2 72 3 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 42 4 4-Methyl-2-(3 - fluorophenyl )pyrim. . . 188 C11H9FN2 076128-66-0 40 Abundance Scan 3420 (23 174 min) 08065 D (-3414) (-) m/z 188.40 100.00% 188

5000

94 22 80 2300 23.20 2340 23.60 43 54 66 80 11 132 0 ' i11" i'11'r '"i '‘f "'i'1'' r ■ byuitfuki । (Hrrteu . ।।11 (11111111 |i 11P 1111 it 111 ilv T 160 III m/z 94.25 15.13% n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826 Anthracene-d10- 188

. --------- 5000 22 80 23.00 23 20 23 40 23.60 m/z 189.40 13.73% 80 94 160 66 17 30 42 52 ■ . 102 118 132 146 .i| 170 18011 | 0V '"I"............................ 11 ■ I ■■111 ■■■ 111uuu —mntmntmm TTTTTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827 Phenanthrene-d10 188 'I ' ■ ' ' I Tidir 22 80 23 00 23.20 23.40 23.60 5000 m/z 184.25 13.66%

80 94 160 30 42 52 66 1 102110118 132 146 ,il 170 181 ' l " " r mIPPTT+ 11 ’ • i»< • n11 *11 ’ • ’ * i * ’ ’ j i111 IJIIlMl" > 111" 111 •n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance . .... ......... . #79716 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 22.80 23.00 23 20 23 40 23.60 91 m/z92.20 9.28% 105 5000 119 65 - n/z-> ........ 4151.. .7 0 TT’fr" 1 ’ " 1 ] 1 1 1 'I 1 । । Ip-'TI I‘‘l l'| I । i'l | । I । III 10 20 30 40 50 60 70 80 146 L ..... . ■ ''11111111'11111'11111r rp-r 90 100 110 120 130 140 150 160 170 180 190 22 80 23 00 23.20 23 40 23 60

08065 .D 041202SCAN.M Tue Apr 16 13:54:45 2002 Page 10

NYC-WTC_000046784

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