GCMS results for sample AE08068, Apr 2002

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Laboratory report documenting GCMS analysis of sample AE08068 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046813–000046840

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 20 Anthracene-dlO- Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T. 23.17 0.35 ug/L 349439 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 86 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 1,4-Naphthoquinone, 2,3-dihydro-... 188 C12H1202 1000157-22-3 40 Abundance Scan 3420 (23 174 min) 08068.D (-3412) (-) m/z 188.35 100.00% 188 I 5000- )...................... 94 40 52 66 80 , 160 22.80 23.00 23.20 23.40 23.60 0 I ' ' 1 ' P' ' ''I । ' H I I . f . । | II I . | I H , | . FrTTTMT . . .......... ........ .. m/z 189.30 18.28% r"■I Tl/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 16 8

5000- 22 80 23.00 23.20 23.40 23.60 m/z 94.20 18.20% e 80 94 160

tVz-> 0Ilt 17 30 42 52 ° I I 102 118 132 146 , 170 1801. I I I ’ I I ; I I I I I I I I I I I I I I 1 I I 1 I I 1 I I 11 I 1 1 I I I I I I I I I I I I I I I I I I 1 I I I 1 I I I I I I I I I 1 " 111111111 1‘N 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TT fl Abundance #79827: Phenanthrene-d10 188 / ‘II ' 22.80 23.00 23.20 2340 23.60 5000 m/z 184.30 13.52%

80 94 160 30 42 52 66 J 102110118 132 146 1 170 181 0. 11U0TTTTTINTTHT TI n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771: 3-Amino-4-methyl-6-methoxyquinoline 18 8 22 80 J ■ i 23.00 23.20 ■ TI....................... I 1 23.40 23.60 m/ z 80.25 9.59% 145 5000-

117 0 I' " ' I' 41 51 63 77 89 102 130 159 173 ------- TTTT I Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40 23 60

08068.D 0412 02 SC7VN. M Tue Apr 16 13:56:54 2002 Page 23

NYC-WTC_000046839

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NYC-WTC_000046839Source: NYC Law Department, mirrored locally

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