GCMS sample AE12676 results, June 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060402\12676.D Vial: 7 Acq On 4 Jun 2002 8:44 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan 15 Library : C:\DATABASE\NIST98.L Peak Number 12 Anthracene-dlO- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

23.06 0.31 ug/L 296557 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 2 Phenanthrene-diO 188 188 3 3-Amino-4-methyl-6-methoxyquinoline 188 C14D10 C14D10 C11H12N2O 001719-06-8 87 001517-22-2 72 1000213-71-3 42 7 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 42 Abundance Scan 3401 (23.062 min): 12676.D (-3393) (-) m/z 188.10 100.00% 188

5000

80 94 158 22.80 23.00 23.20 23.40 43 52 66 0 mmmHmH TTp-n»। ii-i • । 11 [ । 11 11111 । j 11 (< 111 > । 111 * 111 i ■ ■ * * i m/z 189.10 18.29% m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

.................... ................ 5000 22.80 23.00 23.20 23.40 rn/ Z 94.10 17.12% ce 80 94 160 , , 17 30 42 52 7 , 108118 132 146 II 170179 0 TTTTTTTH । ■ | n n|.■ 111.1 ii ।i n 11 ■ ।!■.11■ . ।. i..i-t^i-i'i- ’I m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 rn/z 184.10 15.08%

80 94 160 30 42 52 66 , 132.146 ,|. 170179,1,1 | 11 108118 0-■i ।. 1111 > ■ > > ।. 1.111 u 11U i > । i l l. 1111-1 1111 ■ । [ । H11 ■ ii i 1111 r| 11111111111 TPTTTTTTT nfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline ................... ................. 188 22.80 23.00 23.20 23.40 m/ z 80.10 12.85% 145 5000

41 51 63 77 89 102 117 130 159 173 ............ ...... 1, 0 —mmPTThr ++ rlllm ■ i’ll" ■ rlr ■ । (’’ri ■ 11 rll 11 rt ■ 111'phi 11 r11l 111 Ml । 11’1 iz-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160170180 190 22.80 23.00 23.20 23.40

12676.D 060302.M Wed Jun 05 14:04:48 2002 Page 15

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