GCMS analysis results for sample AE12161, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\ 1 \DATA\052302 12161.D Vial: 14 Acq On : 23 May 2002 8:33 pm Operator: • Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 11 Anthracene-dlO- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.26 ug/L 223480 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 001719-06-8 830)) 188 C14D10 2 Phenanthrene-dlO 001517-22-2 80/ 188 C14D10 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 Benzene, 1-(1-cyclohexen-l-yl) -4... 188 C13H16O 020758-60-5 42 Abundance Scan 3402 (23.068 min): 12161 .D (-3395) (-) m/z 188.10 100.00% 188

5000

94 ,.................... 80 160 22.80 23.00 23.20 23.40 44 66 0 ■ i' “ ‘ i “ ' ■ I" ■' i'1 ” i ■' ‘ ’ i “1 ‘ r “ TPH*mmm i““i m/z94.00 19.77% nfa-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 18.06% 80 16094 , i n 17 30 42 52 66 I I TITu 108118 132 146 ,i| 170179.1 ‘T n/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.00 17.92%

80 94 160 30 42 52 66 , miz-> 1 108118 132 146 ,|, 0'i r> i-itii 111 > 111J i > । I I111 rl I r 111 li TTmTmg 10 2030405060 70 8090 100110120130140150160170180190 179179//... Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 1(8 22.80 23.00 23.20 23.40 m/ z 80.10 13.42% 145 5000

41 51 63 17377 89 102 117 130 . 159 +++-------m 0-Yyrrj. । > 11 < j > > i; ]‘|-i ri’ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12161.D 052202.M Wed May 29 09:54:44 2002 Page 13

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