GCMS analysis results for sample AE12161, June 2002

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Laboratory report documenting GCMS analysis of sample AE12161 conducted on June 5, 2002.

NYC-WTC_000013624–000013642

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052302\12161.D Vial: 14 Acq On : 23 May 2002 8:33 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Thiocyanic acid, 2-benzothi... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

22.54 0.25 ug/L 207181 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Thiocyanic acid, 2-benzothiazoly. .. 192 C8H4N2S2 006011-99-0 42 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 39 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 39 4 cis-2-Methyl-4-phenylthiane 192 C12H16S 076097-69-3/9 Abundance Scan 3312 (22.539 min): 12161 .D (-3301) (-) m/z 192.10 100/00% 192

5000 ..... 96 40 64 82 146 160 22.20 22.40 22.60 22.80 p 0 1—9——mTRHTT 111 “1 'I' “ • i “ “ i “ ‘ ■ i “'' l * “ ■ I ■ • “ i ■ “ ■ i'" ‘ r m/z 191.10 20.15% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

5000 22.20 22.40 22.60 22.80 69 m/z 96.10 16.28% .............. ............ 82 90 108 122 134 148 160 0- . ■ ] > > ■ ■ I > 11 > > > > ] 1-11> > •' ■ i ■ ■

niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- A 192 161 22.20 22.40 22.60 22.80 5000 m/z 146.10 15.27% 77 91 121 149 177 52 64 138

m/z-> 0- ..i T.......... ’’ npm fri ii...... ,,.. nII.... 4111111 i 11 i'l I . . n-rf al,. ..I,... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ‘ I “ '’ I Utt

Abundance #80950:1,5-Naphthalenedithiole 192 2220 2240 22.60 2280/77 m/z 193.00 12.40%

50001 115 128159 40 57 69 79 96 „ 147 0 —— * I *177 1 *■*!'" "I" n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

12161.D 052202.M Wed May 29 09:54:44 2002 Page 12

NYC-WTC_000013640

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NYC-WTC_000013640Source: NYC Law Department, mirrored locally

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