GCMS sample analysis results, AE11906, June 3, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11906.D Vial: 13 Acq On : 22 May 2002 11:36 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 14 Anthracene-dlO- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.26 ug/L 298986 Phenanthranene-dl0 22.92 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Pentacyclo[7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 59 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3402 (23.068 min): 11906.D (-3396) (-) m/z 188.10 100.00% 188

5000

80 94 43 66 160 22.80 23.00 23.20 23.40

miz-> 0-nunmmmtpH ■ i1' ■ ■ i ■ ■ • ■ I" ■ ■ I ‘ ‘ I ■ ■1 ■ i ■ H 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 m/z 80.10 16.63% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 16.03% RR 80 94 160 . 17 30 42 52 66 , 0- ■ i" ■ ■ i ■ TITTTTTHt —108118.132. 146 4170179 — nfa-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 94.10 14.87%

80 94 160 30 42 52 66 11 108118 132 146 I 170179.1,11 0- —** niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)ltetradeca... 188 22.80 23.00 23.20 23.40 m/z 184.10 13.59% 50001 79 91 55 67 105 117 10 131 145 159 , O-mmmpp - IT911141 ‘ t1" ‘ 173.. |l m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23.00 23.20 23.40

11906.D 052202.M Tue May 28 12:13:28 2002 Page 17

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