GCMS analysis report sample AE09517, May 23, 2002

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1 Data File : C:\MSDCHEM\l\DATA\052102\9517.D Vial: 13 Acq On : 21 May 2002 11:07 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 Anthracene-dlO- Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.28 ug/L 284788 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 94— 2 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 4 Phenanthrene-diO 188 C14D10 001517-22-2 40 Abundance Scan 3402 (23.068 min): 9517.D (-3396) (-) m/z 188.10 100.00% 188

5000

80 94 22.80 23.00 23.20 23.40 43 57 66 | 160 I I 0 ‘ I ‘ ‘ I'' " 11 ‘ 1 ‘ I ■''' 1’ • । ■ l • । ■ I |. 11 . 11'1. .! .. ■ >[>>!>! n 111111111 < 1111111111111111111. 11 ‘T m/Z 94.10 16.16% m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

......... ........................ 5000 22.80 23.00 23.20 23.40 m/z 189.10 13.28% . 80 94 _ 160 , , 17 30 42 52 66 , 108118 132 146 ,|| 170179.1 0 ThpmHatt TIWBPmmp ‘T ■n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinolirie 118

145 22.80 23.00 23.20 23.40 5000 m/z 80.10 11.99%

44 51 117 130 63 159 173 77 89 102

miz-> 0 -1+---+-*-------+-+++---+mmmmn 10 2030405060 70 8090 100110120130140150160170180190 II. • i ■"

Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 188 22.80 23.00 23.20 23.40 m/z 184.10 11.99%

5000 102 1,5 145 51 63 75 130 158 ।

m/z—> 0 ----- - t’’4’1 10 2030405060 70 8090 100110120130140150160170180190 | mHmH 22.80 23.00 23.20 23.40

9517.D 052202.M Wed May 22 11:29:28 2002 Page 18

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