GCMS analysis report sample AE09517, May 23, 2002

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GCMS laboratory report for sample AE09517 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013089–000013116

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document

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2 Data File : C:\MSDCHEM\1\DATA\052102\9517.D Vial: 13 Acq On : 21 May 2002 11:07 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 1,2-Phenylene diisothiocyanate Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 22.54 • 0.28 ug/L 285624 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,2-Phenylene di isothiocyanate 192 C8H4N2S2 071105-17-4 50 2 Phenant hrene, 9-methyl- 192 C15H12 000883-20-5 50 3 Bitoscanate 192 C8H4N2S2 004044-65-9 42 4 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 40 Abundance Scan 3312 (22.539 min): 3517.0 (-3301) (-) m/z 192.10 100.00% 152

5000

82 96 146 160 40 52 70 8- 1 22.20 22.40 22.60 22.80

mfe-> 0 .. ।.... ।.... ।. 1.11... . 1111 ij h 11 p 1111111 H 11 u p 111 p 11 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 118 mm ■“I" mall.. m/z 191.00 20.35% Abundance #80862:1,2-Phenylene diisothiocyanate 1912

64 5000 22.20 22.40 22.60 22.80 134 75 90 m/z 193.10 15.45% 39 50 i 107 122 , 148 160 4 0 “i‘H +18.49+4H+H4 . ’ fl1! ri' rl th iThmt ■ i “ “ i ■ ■" i n/z-> 0 10 20 30 40 50 60 70 80 90 1001101201-30140150160170180190200 Abundance #81033: Phenanthrene, 9-methyl- 192

22.20 22.40 22.60 22.80 5000 m/z 146.10 14.46%

......... 29 39 51 63 73 83 ..... 115 126 139 152.165 176.., I, 01 ....... t.... 1.... t.... I... M.... IA , ]T, rl |, 1'1! |.... 1.-j.... [-1... ] Il 111 rh 111 l’l'I'l'i ’’ITT m/z-> • 0 1020304050607080 90100110120130140150160170180190200 Abundance #125827: Bitoscanate 192 -------A---- 22.20 22.40 22.60 22.80 m/z 96.00 14.07% 5000 134 50 63 75 90 160 102 116 0- 4 14 +28 1444 +rHH n 11 rh 111 m > p 148 irH । ■ ■ । |'i M’ 11 > • i ■ ■ ‘ ■ i ' ' i ■ ■ ■ ■ i ■ ’"T n/z—> 0102030405060 70 80 90100110120130140150160170180190200 22.20 22.40 22.60 22.80

9517.D 052202.M Wed May 22 11:29:28 2002 Page 17

NYC-WTC_000013110

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