GCMS sample analysis results for unknowns, May 2002

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Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10131 on May 17, 2002.

NYC-WTC_000046170–000046179

Folder label: “GCMS X 5/7/02 A 5/14/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020513\10131.D Vial: 18 Acq On : 14 May 2002 5:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 1,2-Phenylene diisothiocyanate Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

31.08 0.30 ug/1 32063 Phenanthrene- dl 0 31.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 40 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 36 3 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 33 4 Bitoscanate 192 C8H4N2S2 004044-65-9 33 Abundance Scan 4766 (31.082 min): 10131 .D (-4759) (-) m/z 192.10 100.00% / 192

5000

I I I | I I 1 | I 1 II | ' T I ■ 1 i ' 1 30.80 31.00 31.20 31.40 42 70 86 96 118 136146 160 । i | । i i । | r I । I | । I । I [ । I • I | I I । ) | I i i i | i i I I [ i । । i | I H i | i ) Ti । i i i i । । i i | ] | I I | | | I | I | I i I i । i i । il| i i । I | | I | I [ | I | | | | I I I | I I m/z 191.10 17.06% m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80862:1,2-Phenylene diisothiocyanate 192 A

5000 64 , 1d’’ ...... । । । r r ii । 1........ । । । i j i-r

30.80 31.00 31.20 31.40 75 90 134 m/ Z 194.00 13.03% 39 50 I i1?7 122 4 " r11 11 18.2+HH,4 Ht# rrhd..... . 11'1 TT 148 160 p1" । m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80950:1,5-Naphthalenedithiole 192

30.80 31.00 31.20 31.40 5000 m/ z 96.20 12.17% 115 128 159

40 57 69 79 96 147 1111111111111111 ri । ll । mdrdlrrppmerHmmRM r I 1,1' 'pi'. 11 "'llp +111/177 1 ■ 111 /z-> Abundance 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 1 >2 14.... ) — 30.80 31.00 31.20 31.40 m/ Z 94.00 11.13% 147 5000 45

m/z-> 111' ‘" i"11P 27 i ‘ HHHHH I I 82 9 115 -H #--- 58 69 134 158 177 mm 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 4 ... 1,111..... 1 30.80 31.00 31.20 31.40

10131.D SCAN020507.M Tue May 14 16:00:20 2002 Page 4

NYC-WTC_000046177

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GCMS sample analysis results for unknowns, May 2002 · Box DEP Box 25

NYC-WTC_000046138

Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10068 on May 17, 2002.

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