GCMS analysis page for sample AE11569, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11569.D Vial: 22 Acq On : 22 May 2002 5:06 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Thiophene, 2-[2-(3-thienyl)... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.29 ug/1 30754 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 47 2 5-[5-Methylfurfurylidene]hydantoin 192 C9H8N2O3 1000214-69-2 47 3 1,2 -PHenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 47 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 43 Abundance Scan 4768 (31.094 min): 11569.D (-4757) (-) m/z 192.10 100.00% 192

\ 5000

l-r i 1 1 ' 1 I

O-T 44I,’ id84118 160 , , i — —P ' I ' ' ‘ ' i ' ' ' ' I ' ' ' ' l 415 1 ' 30.80 31.00 31.20 31.40 m/z 191.20 24.47% nz-> 0 50 100 150 200 250 300 350 400 Abundance #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 1$2

147 5000 30.80 31.00 31.20 31.40 45 m/z 83.95 16.45% . 69 96115 o1 26, tthydaql/ 1 4— .............. ............................... m/z-> 0 50 100 150 200 250 300 350 400 Abundance #80918:5-[5-Methylfurfurylidene]hydantoin 121 1912

30.80 31.00 31.20 31.40 5000 m/z 193.20 15.59% 43 79

O—T -L 1 1 100,1,149.1.............. m/z-> Abundance 0 50 100I 150 200 250 300 #80862:1,2-Phenylene diisothiocyanate 192 350 400 .A. H.. 30.80 31.00 31.20 31.40 m/z 96.00 15.17% 64 5000

90 134 1 39 0 —18LL.1k..1109..1 160 I.................................. 1 ' ■ T I ' r ' ' 1 1 ' ' ' I—I l I > -1 > > I 1 n/z-> 0 50 100 150 200 250 300 350 400 30.80 31.00 31.20 31.40

11569.D SCAN020521.M Fri May 24 09:44:09 2002 Page 4

NYC-WTC_000025599