Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.
NYC-WTC_000048148–000048168Folder label: “GCMS X 4/9/02 A 4/19/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C : \DATABASE\nist 98.1
Peak Number 5 Thiocyanic acid, 2-benzothi... Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T. 31.09 0.32 ug/1 639852 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 59 2 4H-l-Benzopyran-4-one, 5,7-dihyd... 192 C1OH804 001013-69-0 42 3 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 42 4 Bitoscanate ______________________________ 192 C8H4N2S2 004044-65-9 40 Abundance Scan 4768 (31.094 min): 08425.D (-4753) (-) m/z 192.10 100.00% 192
5000 40 ............ ...... ..............
m/z-> 51 ■ i" " ।" Tggrtr 74 118 82 96 | 160 146 400 I|M । 1 11 I Tr 111 (>> r 1111111»r i i (> I 111, i /1111111! 1111111 ■ 111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 „ll— 30.80 31.00 31.20 31.40 m/ Z 40.10 26.80% Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192
5000 30.80 31.00 31.20 31.40 m/z 191.10 17.59% 45 “1 90 198 122 134 148 160 n/z-> TI P Tmmmm 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 111rr
Abundance #80873: 4H-1 -Benzopyran-4-one, 5,7-dihydroxy-2-methyl- 192
30.80 31.00 31.20 31.40 5000 m/z 193.10 16.42%
39 69 o 124 152 164 144450,59, 82 96 m | 135 | ■*' I " "Mi l I I I | i rl i | > ! I I |'l I I ! |‘i'l I I | I I'l I | I I rt | I'l I I | IHTTT MINIIp 111IT n/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 1 2 ...../A,... . 30.80 31.00 31.20 31.40 m/ z 96.00 12.89% 147 5000 45 | 58 69 134 -2-Hl++ 82rr’palu96,05115 M rl । | । r 111 i'i 1 58.,177 ‘I 111 "11" 1111111 I T8 A TT /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40
08425.D SCAN020418 .M Thu May 02 15:28:10 2002 Page 7
NYC-WTC_000048158
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NYC-WTC_000046864
Laboratory report documenting GCMS analysis of sample AE07766 including surrogate recovery and unknown compounds on April 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048121
Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048355
GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048106
Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048134
Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047926
GCMS analysis report for sample AE08258 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048287
Initial analysis page for sample AE08261 showing surrogate recovery data and unknown compound screening.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048401
GCMS analysis report for sample AE08266 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048378
GCMS analysis report for sample AE08265 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047886
GCMS analysis report for sample AE08256 showing surrogate recovery and unknown compounds from April 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047802
Laboratory report documenting GCMS analysis of sample AE08252 conducted on April 19, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048309
GCMS analysis report for sample AE08262 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000048081
Department of Environmental Protection GCMS analysis record dated April 9-19, 2002.
Filed in the same folder
NYC-WTC_000048082
Fragmented document page containing metadata and identifiers related to GCMS testing procedures from early April 2002.
Filed in the same folder
NYC-WTC_000048085
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.
Filed in the same folder
NYC-WTC_000048094
Laboratory report of GCMS calibration (Sample AE08323) conducted between April 9 and May 3, 2002, showing response factors for volatile organics.
Filed in the same folder
NYC-WTC_000048098
Laboratory report of GCMS reference standard run (Sample AE08323) conducted between April 9 and May 3, 2002, verifying instrument performance.
Filed in the same folder