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GCMS analysis results for sample AE08431, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048121–000048133

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048130
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08431.D vial: 18 Acq On : 20 Apr 2002 12:52 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Thiocyanic acid, 2-benzothi... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

31.09 0.35 ug/1 755897 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 53 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 42 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 42 4 Bitoscanate 192 C8H4N2S2 004044-65-9 40 Abundance Scan 4767 (31.088 min): 08431 .D (-4757) (-) m/z 192.10 100.00% 192

5000

40 on 96 146 160 1 .... A..... 30.80 31.00 31.20 31.40

m/z-> " | । ! I | . . . I | I I I I | 49 70 82 I I l‘[ I I l l| i ll ! | ! f

10 20 30 40 50 60 70 80 90 100110 120 130140150 160170180190 200 I ! I | I 120 yulryunl;....... -m Tr m/Z 191.00 16.26%

Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

5000 T 30.80 31.00 31.20 31.40 m/ z 40.10 11.65% I5 ,90 118 122 134 148 160 I‘ ‘ I *'1 ‘ I Tmpmmmmmmmmmmpm ‘ ‘11 m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140150160170180190 200 Abundance #125822:1 3-Benzodioxole, 4-methoxy-6-(2-propenyl)- 192

30.80 31.00 31.20 31.40 5000 m/z 96.20 10.58% 91 165

n/z-> Abundance 15 27 । mpmmr-HHHH 39 70 65 77 53

10 20 30 40 50 60 70 80 90 100110120 130 140150 160170180190 200 #80895:1.3-Benzodioxole, 4-methoxy-6-(2-propenyl)- 103 119 131 147 , mu .... ........ U., 11111111 TTT

192 30.80 31.00 31.20 31.40 m/z 146.10 9.99% 5000 91 165 39 51 65 7 103 119 131 77...I1 1 ’ I 147 --HHHH11,1 1' HI " " I" " IL /z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170 180190 200 30.80 31.00 31.20 31.40

08431.D SCAN020418.M Thu May 02 15:40:29 2002 Page 6

NYC-WTC_000048130

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NYC-WTC_000048130Source: NYC Law Department, mirrored locally

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