GCMS analysis results for sample AE08431, May 2002

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Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048121–000048133

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08431.D Vial: 18 Acq On : 20 Apr 2002 12:52 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C: \MSDCHEM\1\METHODS\SCAN020418 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

31.96 0.34 ug/1 725655 Phenanthrene- dl 0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dl0 - 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 53 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 47 Abundance Scan 4915 (31.957 min): 08431 .D (-4905) (-) m/z 188.10 100.00% 188

5000

80 94 TT | ' • <T | » I ' ’ • • | •

miz-> ‘i 1 1 ' 1 1 1 1 1 1 I 40 | 54 66 TTTNT । 132 146 158 THT ' " 111" r " ' i " " i ■ " 11fl" r11111111111" 111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 „l 31.60 31.80 32.00 32.20 m/ Z .94.10 19.92% Abundance #79826: Anthracene-d10- 188

5000 Ti | ■ 1 '’T । . . . . t ' . ' ' | . 31.60 31.80 32.00 32.20 m/z 80.10 17.66% 80 94 160 , . 17 30 42 52 66 108 118 132 ■i""i ■ Iu 1111111111" -HH TTTTT ‘1 146—44179179 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 15 I ' ‘ TT I < . I I I . . 1 1 , . 31.60 31.80 32.00 32.20 5000 m/ Z 189.10 15.81%

80 94 160 30 42 52 66 . 11 108 118 132 146 ,|.| 170179,1,1 '11" 'I " " I" " I" " I11" 111'' I " 1,1 111 +TTmmmm m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821: Selenide, ethyl 1 -methyl-1 -penten-3-ynyl TT IFTI4ss"II‘II1" 188 31.60 31.80 32.00 32.20 m/Z 184.10 13.32%

5000

79 145 159 173

/z—> ‘I ‘ 7 I 1 1 1 1 I 1 1 I 1 I 1 1 1 ' I J 1 1 1 j ' I ' 1 ] ' 1 91 107 119 131 J . m I' 11' 111111 rin 11 111111'1'11 T 1' 111'' —— 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

08431.D SCAN020418.M Thu May 02 15:40:31 2002 Page 7

NYC-WTC_000048131

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GCMS analysis results for sample AE08426, May 2002 · Box DEP Box 27

NYC-WTC_000048169

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

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