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GCMS Analysis Results, Sample AE08261, April 22, 2002

Machine-extracted title · confidence 100%

Initial analysis page for sample AE08261 showing surrogate recovery data and unknown compound screening.

NYC-WTC_000048287–000048308

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048303
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08261.D Vial: 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Anthracene-dlO - Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 23.18 0.57 ug/L 1078580 Phenanthranene-dl0 23.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 94 2 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 58 3 Phenanthrene-diO 188 C14D10 001517-22-2 52 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 50 Abundance Scan 3420 (23.174 min): 08261.D (-3412) (-) m/z 188.10 100.00% 1(8

5000

80 94 vT 22.80 23.00 23.20 23.40 23 60 O-T 42 TmH । t*i i j‘| T 57 66106 132 pihef... .| fM1, ■ ■■. 158 180, m/ z 18 9.10 16.09% n/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 abundance #79826 Anthracene-d10- 188

5000 22 80 23.00 23.20 2340 23.60 m/ z 94.05 15.43% 80 94 160 17 30 42 52 66 . 102 118 132 146 1 170 180 . 0 *WUum—ug—hn---HH tgtt T‘1r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl 168 /.,...........................

22 80 23.00 23.20 23.40 23 60 5000 m/z 80.05 14.38% 79 145 159 91 107 ng 131 173

n/z-> 0 ■ 11' > > ।'1 > 11 > < " । ' 111' > । । । । ll44 ■ । 11 i r / > । | |■i'lll‘| i rep i i r

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 22 80 23 00 23 20 23.40 23.60 m/z 184.05 13.94% 5000

80 94 160 30 42 52 66 Tl/z—> 0 p-rrrp-r 11"■ 'i""i11"i'11'i"11 "111 .I 102110118 132 146 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 44170.180——. 22.80 23.00 23.20 23 40 23.60

08261.D 041702SCAN.M Thu Apr 18 09:47:23 2002 Page 13

NYC-WTC_000048303

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NYC-WTC_000048303Source: NYC Law Department, mirrored locally

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