GCMS sample AE11154 analysis with surrogate recovery, May 2002

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Data File : C:\MSDCHEM\l\DATA\020515\11154.D Vial: 20 Acq On : 16 May 2002 6:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Anthracene -dlO- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.32 ug/1 33335 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 72 2 Phenanthrene-d10 188 C14D10 001517-22-2 72 3 Pentacyclo[7.3.1.1. (4,12) . 0 (2,7) . . . 188 C14H20 1000215-61-8 53 4 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 45 Abundance Scan 4913 (31.946 min): 11154. D (-4906) (-) m/z 188.15 100.00% KB

5000

94 160

mfe->______ 20 43 54 66 78 40 60 80 --P—100 120 140 160 180 1 'T' । । । | । । 200 220 234 | 31.60 31.80 32.00 32.20 m/z 189.10 18.63% Abundance #79826: Anthracene-d10- 188

5000 1.T IItt 1"i I I I I I I 31.60 31.80 32.00 32.20 m/ Z 160.20 18.54% rr 80 94 160 1728.40,52,4141106118.132 146.— +---+H n/z->______ 20 40 60 80 100 120 140 160 180 200 220 Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/z 184.10 17.87%

80 94 160 ' ’ 1 1 28,40,52,66.1 ,| 108 120132 146 J......... .............. ' 11111'!' r> i i । । i i 11 i i r । 1TI । । । 1 i ■ ' 1 1 i m/z—> 20 40 60 80 100 120 140 160 180 200 220 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )]tetradeca... ' ' | r ' ' ' | ।T | । i । ' | | ' । i | | 188 31.60 31.80 32.00 32.20 m/z 94.20 13.56% 5000 79 91 55 67 10E 131 105117 1 145 159 173 Il...... n/z—> ‘ 1 I ' 20 40 60 80 --4 — 100 120 140 160 180 200 220 • ■ i ' ■ ' ■ i ■ ' ■ 1 i 31.60 31.80 32.00 32.20

11154.D SCAN020507.M Thu May 16 14:37:47 2002 Page 7

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