GCMS sample AE11154 analysis with surrogate recovery, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11154.D Vial: 20 Acq On : 16 May 2002 6:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 3-Eicosene, (E)- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 36.44 0.66 ug/1 60628 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Eicosene, (E)- 280 C20H40 074685-33-9 52 2 9-Eicosene, (E)- 280 C20H40 074685-29-3 52 3 3-Octadecene, (E)- 252 C18H36 007206-19-1 52 4 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 50 Abundance Scan 5678 (36.441 min): 11154.D (-5667) (-) m/z 83.10 100.00% 41 57 83 69 97

5000

111 125 161 4 “hk hl 36.20 36.40 36.60 36.80 ' I " " I 1 1 "Oid I ,I I I I . ........... J ...................................... 264....... m/z 41.10 96.50% nz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #16986: 3-Eicosene, (E)- 43 57 83 97 5000 70 29 111 36.20 36.40 36.60 36.80 m/z 57.10 91.96% 125 280 +74, '-r TIB +rT 1 13% 153 167 182 196 210,224 .252 TT m/z-> 20 40 60 80 100 120 140 160 180 . 200 220 240 260 280 Abundance #16761:9-Eicosene, (E)- 43 $7 83 97 WMelu 36.20 36.40 36.60 36.80 70 5000 m/z 55.10 90.99% 29 111 125

miz-> — —1IT 20 40 60 U 80 100 I 139 153 168181 196209223 120 140 160 180 200 220 240 252 260 280 280 Abundance #22895: 3-Octadecene, (E)- 4 55 69 36.20 36.40 36.60 36.80 83 m/ Z 69.10 78.48% 97 5000 111 27 | I 125 _

m/z—> '2011 404+T60Tr 80 100 252 J l h 139 154 168 182 196209 224 PPP 120 140 160 180 200 220 240 260 280 4 36.20 36.40 36.60 36.80

11154.D SCAN020507.M Thu May 16 14:37:50 2002 Page 8

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