GCMS analysis results, Sample AE08266, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial: 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 7 Eicosane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

21.82 0.21 ug/L 364192 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane 282 C20H42 000112-95-8 90 2 Eicosane 282 C20H42 000112-95-8 86 3 Pentadecane 212 C15H32 000629-62-9 86 4 Eicosane 282 C20H42 000112-95-8 86 Abundance Scan 3190 (21 822 m:n): 08266.D (-3180) (-) m/ z 57.10 100.00% 57

43 71

5000 85 A n/z-> 04 ■ ■ i'11' r 20 40 J , L. 11 60 99 113 | I 0-1 .r/I" * r | | r 80 100 140 120 "l40 "l60 180 "206 "220 ' 240 260 ' 280 ' 21.40 21.60 21.80 22 00 22.20 m/ z 71.10 69.08% Abundance #112343: Eicosane 43 57

5000 71 A.. 85 21.40 21 60 21.80 22 00 22.20 29 m/z43.10 64.15%

04 ll J +4 - j9 113 127 141 155 .......... . •n/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #112344' Eicosane 7 43 71 21 40 21.60 21 80 22 00 22 20 5000- m/ z 85.10 39.61% 85 29 99 01 1,4442 +L 4,1 ,143,127 141 155 169,183 197 211 225., 282 n/z-> Abundance 20 40 60 80 100 120 140 160 180 #16493 Pentadecane 200 220 240 260 280 4.. "... 43 57 21 40 21.60 21 80 22 00 22.20 m/ z 41.10 35.12% 71 5000 85 29

0 15 | JI 1*.* 99 113 127 141 155 169 183 212 M..P./ nd I ■ r i | | ■ ■ ■ ■ | | | I . | ■ I I I ■ i I . ; 1 I I ■ I . MAPAAMRMMAAAA —MAAMAAAA /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 21 40 21.60 21.80 22 00 22.20

08266.D 041702SCAN.M Thu Apr 18 09:59:57 2002 Page 12

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