GCMS analysis results, Sample AE08266, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial: 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Phenanthrene, 9-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.35 ug/L 610825 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 64 2 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 42 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 42 4 Anthracene, 9-methyl-___________________ 192 C15H12 000779-02-2 42 Abundance Scan 3329 (22 639 min): 08266.D (-3319) (-) m/z 192.10 100.00% 19 2

5000

' 1 i ' • I • • ' • I ' • 160 96 146 22 40 22.60 22.80 23 00

n/z-> 01 40 1111" ।' " 'I'1'" I"'' — 70 82 52 HHHH 120 I TTTTTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 e. TTH - m/z 191.10 I 17.64% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 .... P . . 22 40 22 60 22 80 23 00 m/z 193.00 14.04% 96

Tl/Z-> 29 39 51 63 7 5 83 0+ ' i " " i ■ " ■ r " ■ i ■ 1 115 126 1 39 1 52 TTTTTTTTTTW*TWWTWWTIWWIWTTTTT*T 165 Jr 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 176 TTTTTT 41 Abundance #81041. Phenanthrene, 3-methyl- 152 1 ■ i ■ 1 T-r-p-r 2240 22 60 22.80 23.00 5000 m/ z 96.00 13.69%

96 AE 27 39 51 63 74 82 | 115 126 139 152 0 176 0+ 11'1111" " i'1" I'1 ■ । i'i 1111 ri i i rh ’ II r‘.........11 ri 11111111111*| । > 11 tri "I i‘i 1111111111 /I Tp n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methy- I 192 2240 22 60 22 80 23.00 m/z 146.10 13.53%

5000

96 AE . 27 39 51 63 74 82 1 115 126 139 152 100 178 . 0 TITT j 11 ITTEMTT |*i 11 t"| Tri 111 i‘l 1 rI’r fl'| । Pl । । । 1111 iti 11 111 T| ri । i'| 1 । । । |I. । । । Ji 11 । 11 H 111 /I 1111 . । 11 Tl/Z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.40 22.60 22.80 23.00

08266.D 041702SCAN.M Thu Apr 18 09:59:58 2002 Page 13

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