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GCMS analysis results, Sample AE08266, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08266 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048401–000048420

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048418
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial: 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.58 ug/L 1003020 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 94 2 Phenanthrene-dlO 188 C14D10 001517-22-2 78 3 Cycloheptanone , 4-phenyl- 188 C13H160 067688-28-2 50 4 Pentacyclo[7.3.1.1. (4,12) .0(2,7) ... 188 C14H20 1000215-61-8 39 Abundance Scan 3420 (23 174 min): 08266.D (-3414) (-) m/z 188.10 100.00% 1(8

5000

80 94 57 22.80 23 00 23 20 23.40 23.60 -. 66 — 43 ,102 132 146 158 | 0-P---------- mPmPmT TT) m/ z 189.10 16.27% n/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #79326 Anthracene-d10- fl 188

5000 22 80 23 00 23 20 23 40 23.60 m/z 94.05 16.26% 80 94 160, 66 17 30 42 52 . 102 118 132 146 ,11 170 180 , 0- I ■ ■ 1 ■ I 1 1 " I 1 > 1 1 I 1 1 1 1 I • t i '1111' 11'111" '1111'111" ' i' ■1111 ihi ■'' I ■' ■' I 'I'"1111' n/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 168

22.80 2300 '23 20 23 40 23.60 5000 m/ z 80.10 15.55%

80 94 160 i1!

n/z—> 30 42 52 66 1 102110118 01 | । । । rT I | I I , ! | I I I I | I I I I | । I I । | । I I'! | I THTt 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 146 1 170 180 m Abundance #79739: Cycloheptanone, 4-pheny- 108 22 80 23 00 23 20 23.40 23.60 117 104 m/ z 184.10 11.52% 91 160 5000 131 170 27 39 51 65 78 145 iln.lili 0 T-p-m-p-r —+++++ ‘h’" “p-TT i-p-r Tm /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23 20 23.40 23.60

08266.D 041702SCAN.M Thu Apr 18 09:59:58 2002 Page 14

NYC-WTC_000048418

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NYC-WTC_000048418Source: NYC Law Department, mirrored locally

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