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GCMS results for sample AE08069, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046841–000046854

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08069.D Vial : 26 Acq On : 16 Apr 2002 7:13 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.28 ug/L 289560 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87 2 Phenanthrene-dlO 188 C14D10 001517-22-2 50 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3420 (23 174 min) 08069.D (-3414) (-) m/ z 188.4 0 100.00% 168

5000

80 94 22 80 23 00 23 20 23.40 23.60 136 156 -mTPT m/z 94.25 16.84% nz-s 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826 Anthracene-d10- 188

5000 22.80 23.00 23 20 23.40 23.60 m/z 184.30 15.52% RR 80 94 160 . 17 30 4 2 52 00 | | 102 118 132 146 1 170 1801. 0^ ।! । 11 11 i 1 । ] । rrrrl I । 11111 111 I I । | 111 | | 11 i t | | 11 i | । 111 । । । n 11 । 11 । | । । 11 i । f i 11 ; . .... . 11 1 1 | ttr 11 । n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827' Phenanthrene-d10 188 4—M 22 80 23 00 23 20 2340 23.60 5000 m/ z 18 9.40 14.99%

80 94 160 30 42 52 66 .1 102110118 132 146 | 170 181 0 । ri! "IrR 11 i i i > | i i i i 1111 111 I 11 111 1'1 11 > । I | H 1 ■ | I " ‘ | I I ' > | I I " | I I I ■ | ■ I ' | > >Tl'|... . n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 108 22 80 23.00 23.20 23.40 23 60 m/ Z 80.20 12.92%

5000 102 115 145

51 63 75 94 130 158 0 IPPPT ,,11 ‘I'.. I... |.. 11J ” 111" '1111'' 1 1' I I ’ I 1I 1. TPTTTT T’T Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23.00 23.20 23.40 23.60

08069.D 041202SCAN.M Tue Apr 16 13:58:31 2002 Page 9

NYC-WTC_000046853

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NYC-WTC_000046853Source: NYC Law Department, mirrored locally

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