GCMS analysis results for sample AE08063, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08063 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046740–000046756

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020415\08063 .D Vial: 20 Acq On 16 Apr 2002 2:21 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 9 Anthracene-dlO - Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.39 ug/L 538795 Phenanthranene -dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 (2) Phenanthrene-dlO 188 C14D10 001517-22-2 72 3 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 50 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3420 (23 174 min): 08063 D (-3414) (-) m/z 188.40 100.00% 188

5000

80 94 159 22 80 23 00 23.20 23.40 23 60 40 54 66 | .1 132 146 150 0 11 "rl1 nrrrtti > 11 ■ r 111 ■ ■ f 11 < । H ■ 11 ■ j H i ■ 11 ■ । ■ । FTTI mtThTHHI 111 ii 111> r1" i m/z 189.35 13.63% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826'Anthracene-d10- 188

5000 ( J — ( ( 22 80 23 00 23 20 23.40 23.60 m/z 94.3 0 12.74% 80 94 160 1. 66

n/z-> 0- | । t|~, 17 30 i| II, mH 42 52 1. . 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 118 132 146 | 170 180 . TrTrnTt 1111111111 " 111111111 H"h 1111 j

Abundance #79827 Phenanthrene-d10 188

22 80 23.00 23.20 23.40 23.60 5000 m/z 184.30 12.22%

80 94 160 30 42 52 66 04 I..... I ■ ■ ■ ■ 11 ■ ■ ■ I I t 111.11.1». I-I 111,102119118 ,. 132 , | i1,46,, 4,170, 1891 11 n/z—> 10 20 30 40 50 60 70 SO 90 100 110 120 130 140 150 160 170 180 190 Abundance #79744: 4-Methyl-2-(3-fluorophenyl)pynmidine TIF 188 22 80 23.00 23 20 2340 23.60 m/ Z 80.30 9.16% 5000 121

67 QA 173 39 50 I, 75 if 102 | 134 146 161 | 0 i1 " ■ i' " 11'1" P111 r111111 " ।> 1111 Pi । p 11111 1 ■ ■ P'' " 111 ■ ' i i ■ I ' 11 " । p'' 11 ' 1111" '1 r I TIT n/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 2340 23 60

08063.D 041202SCAN.M Tue Apr 16 13:51:59 2002 Page 12

NYC-WTC_000046755

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