GCMS analysis results for sample AE07978, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE07978 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046707–000046721

Folder label: “GCMS X 4/5/02 A 4/16/02”

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Data File : C:\MSDCHEM\1\DATA\020415\07978.D Vial : 18 Acq On : 16 Apr 2002 12:44 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.44 ug/L 592338 Phenanthranene- dl 0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

0 Anthracene-dl0 - Phenanthrene-dl0 4-Methyl-2-(4 -fluorophenyl)pyrim... 4 2-Quinolinecarboxaldehyde, 8-hyd. . . Abundance Scan 3420 (23.174 min) 07978.D (-3414) (-) 188 188 188 188 C14D10 C14D10 C11H9FN2 C10H8N2O2 001719-06-8 90 001517-22-2 56 076128-67-1 42 005603-22-5 42 m/z 188.40 100.00% 108

5000 .......... / 94 ■ । 1 ■ ■ ' । ■ Tilt ' • ' l 1 ' IPITT . 158 22 80 23.00 23.20 23.40 23.60 42 54 66 80 146 ,h 180 0 mmmmmmmmpm 1111 H 111" 11111|11 / ' I" lq'" " ।...' | AV 1’111 I. m/z 94.25 16.72% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22 80 23 00 23 20 23.40 23 60 m/z 189.40 16.37% 80 94 160 i I 66

n/z-> 17 30 42 52 0 ........... IInnptnpt + l ,| 102 | "■ 111 | 118 132 146 11, ...... . ................ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 +4170.180— Abundance #79827 Phenanthrene-d10 188 ......... ' I 1 ' ' ' I I ’ ' ' 1 I ' 22.80 23 00 23.20 23.40 23.60 5000 m/z 184.30 13.87%

80 94 160 30 42 52 66 1 102110118 132 146 1 170 180 Qi1IWPTTCTTTTTTHTTH I I " 11 11 | | I i 11 11 ri । [ I 1111 n 11 11 rfr ■ 11 | ' i 11 | I’lTI mu n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79745: 4-Methyl-2-(4-fluorophenyl)pynmidine 188 22 80 23 00 23 20 23.40 23.60 m/z 158.30 9.86% 121 5000 173 67 94 39 57 । 75 84 I 102 133 146 i •' ■ 161 .......... / 0 '| | । 1 "| " । 11 ■ I i । ' ii |' 'll । । । । । 11 ■ , I ■ ■ ■ ( < । ■ I ■ ■ i''' ■ i ■ • ■ ■ i ■ I ■ ■ ।. T’T ' I 1 ' ' 1 I rr ‘ ' 1 I 1 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40 23.60

07978.D 041202SCAN.M Tue Apr 16 13:47:48 2002 Page 10

NYC-WTC_000046720

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GCMS results for sample AE08069, Apr 2002 · Box DEP Box 27

NYC-WTC_000046841

Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.

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