GCMS analysis results for sample AE08324, May 2002

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Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048134–000048147

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08324.D Vial: 11 Acq On : 19 Apr 2002 5:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.37 ug/1 808745 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dl0- 188 C14D10 001719-06-8 91 Phenanthrene-dl0 188 C14D10 001517-22-2 38 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 36 4 Pentacyclo[8.4.0.0(3,7) .0 (4,14) . .. . 188 C14H20 1000099-27-2 36 Abundance Scan 4915 (31.958 min): 08324.D (-4903) (-) m/z 188.15 100.00% 188

5000

80 94 1 1 i r ' 1 ; i 1 ■ ‘ 1 1 1 1 1 1 1 1 1 1 1 1 1 160 31.60 31.80 32.00 32.20 44 54 66 ’Tt—111111013111B0110010110011000TT—001—TTET ■ l•• ■ ■ । , il 132 111 ■11• ......iil|l । | । i । I | I 1 r I [ | I m/z 184.10 16.18% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1818

5000 1I !’’IIIIIIIIIIIII 31.60 31.80 32.00 32.20 m/z 189.20 15.95% 80 94 160 , , 17 30 42 52 66 1 r' " i11" i'1" i1" 1111" 111111 + 108118 132 I I I I I IT" I I I I I I I I I I I I 146—4179179 , m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/ z 94.10 15.59%

80 94 160 30 42 52 66 . I 108 118 132 146 11 170179.1,1 | ■ | i ' I ■ | I I I I | I । । < p i I I | I II I | I I I I | I1 I1 111 11 t [ 11 I 11 ri ri ।»1 11 11 11 T!Ti> 1111 rl I ‘i 111111111 tn । TTT n/z-> 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 31.60 31.80 32.00 32.20 m/z ,80.20 14.11% 145 5000

41 51 63 77 89 102 117 130 159 173 tt/z-> ---------- -pilin..... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I ■ ■ i ' ' ' ' i 1 r 1i ■ 1 1 1 'i 1 1 1 1 i 1

31.60 31.80 32.00 32.20

08324.D SCAN020418.M Fri May 03 09:04:40 2002 Page 8

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GCMS analysis results for sample AE08323, May 2002 · Box DEP Box 27

NYC-WTC_000048106

Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.

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