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Document fragment from DEP Box 27, April 2002

Machine-extracted title · confidence 80%

Single page document fragment from the DEP Box 27 archive folder dated between April 10 and April 15, 2002.

NYC-WTC_000048683–000048692

Folder label: “GCMS X 4/10/02 A 4/20/02

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Scanned page image, NYC-WTC_000048691
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08489.D Vial: 26 • Acq On : 20 Apr 2002 8:45 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 678368 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 001719-06-8 59 188 C14D10 2 Antipyrine 000060-80-0 47 188 C11H12N2O 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 38 4 Antipyrine 188 C11H12N20 000060-80-0 38 Abundance Scan 4915 (31 957 min): 08489.D (-4906) (-) m/z 188.20 100.00% 188

5000 40 94 80 ‘d 1FTI‘‘SI*4I1I

niz—> TWWIBImputr 51 66 TTPHTHTro 136146 160 TIm——maDHag 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ml 31.60 31.80 32.00 32.20 m/z 40.10 31.99% Abundance #79826: Anthracene-d10- It®

5000 ' i 1 ■ ■ • i 1 ‘ ■ i ■ • • ■ i 1 ‘ 1 1 I 1 31.60 31.80 32.00 32.20 m/z 94.10 24.08% RR 80 94 160 I, 17 30 42 52 P „ 108118 132 146 N 170179 T11 11 in 111i1i111i11IIII1111 H 11 111 lill| H i11 111 1111 n | n11 [I 11i1 n 11111 Tsli 11 n i "I’l’l’t mi miz-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #79725: Antipyrine 188 TI — , IT | . . ! I | I ! I | | 1 96 3160 31.80 32.00 32.20 5000 m/z 189.20 14.75% 77 56 105 27 39U I, .1. 67 .„ . .|| 115 130 145 159 173 _ 1 rnfz~> rrp> •■ 1n j1111I ।■ r• |’’ ’ I r 11 np 11u 111’l 11 l r 11'| 1111111 n i r ■111 'tI ‘ ‘ ‘ ‘ I ‘' ’r ''111‘ r’ Tt 1 ‘ I11t‘ r’ l r l’’tr : 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... KB 31.60 31.80 32.00 32.20 ‘ ‘ ‘ ' m/z 80.05 13.40% 5000 79 91 55 67 131 117 miz-> l “1' I “ “ I “ “ 11' 4 10 2030405060 70 8090 100110120130140150 160 170 180 190 Ju * 31,60 31.80 32.00 32.20

08489.D SCAN020418.M Thu May 02 12:04:01 2002 Page 5

NYC-WTC_000048691

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NYC-WTC_000048691Source: NYC Law Department, mirrored locally

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