GCMS analysis results sample AE08486, May 2002

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GC/MS analysis report for sample AE08486 conducted May 7, 2002, detecting unknown compounds and surrogate standard 2,4-DDD.

NYC-WTC_000048635–000048646

Folder label: “GCMS X 4/10/02 A 4/20/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08483.D Vial: 20 Acq On : 20 Apr 2002 2:50 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.34 ug/1 732285 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 59 2 Cycloheptanone, 4-phenyl - 188 C13H160 067688-28-2 37 3 Phenanthrene-diO 188 C14D10 001517-22-2 37 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 33 Abundance Scan 4914 (31.952 min): 08483.D (-4901) (-) m/z 188.15 100.00% 188

5000

40 94 1’T i ■ ■ 1 1 i 1 1 1 ' I ' 1 1 1 I 1 80 31.60 31.80 32.00 32.20 54 66 132 146 158 170 mth T| > • > 11 > 11 I 11 1 TITTPTPTp ■p-l-r m/z 40.10 20.80% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 MWyPyWYWW” Abundance> #79826: Anthracene-d10- 1118

5000 31.60 31,'so 32.00 32.20 ' ' 1 ' m/z 94.10 20.14% 80 160 , I94 17 30 42 52 66 miz-> | J 108118 132 146 IUpn—uap—nnn—hur ylagiril 1141111184112211/227782411424122241 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Ttttt +4179179. Abundance। #79739: Cycloheptanone, 4-pheny- 188 117 104 ’I । । V । , , — * 91 31.60 31.80 32.00 32.20 160 5000i 131 m/z 184.10 15.18% 170 27 39 51 65 78 145 poip 11 ■ ■ h ■ ■ pi t Mrp l i-i nl , Iil,, ।, ll, , All ,, ill, ।, J, l re ,. ।., lIT-uur ,, mz-> 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 i ‘ ■ 1 i ■ 1 ' 1 i ' 118 31.60 31.80 32.00 32.20 m/z 189.05 14.06% 5000

80 94 160

miz—> 30 42 52 66 1+108118..132.146.4.170179/—.. 171 . I I I ! I I I ! IT II I I I I , | I 1 I . I ! I I I | I . |-| | I n I | | I, I | 1 |~! | | l f, i | ■ l ! , I I ! | | I ,, | r, | rl’l’i i i nii [TlHI’r , , 10 20 30 40 50 60 70 80 90 100110120130140150160170 180 190 . . | /. . T I . . I I J . . , . | . I I | | |

31.60 31.80 32.00 32.20

08483.D SCAN020418.M Thu May 02 11:45:03 2002 Page 7

NYC-WTC_000048645

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GCMS sample analysis report AE08483, May 7 2002 · Box DEP Box 27

NYC-WTC_000048623

Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.

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