NYC-WTC_000048623
Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 12 pages
GCMS analysis results sample AE08486, May 2002
Machine-extracted title · confidence 95%GC/MS analysis report for sample AE08486 conducted May 7, 2002, detecting unknown compounds and surrogate standard 2,4-DDD.
NYC-WTC_000048635–000048646Folder label: “GCMS X 4/10/02 A 4/20/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08483.D Vial: 20 Acq On : 20 Apr 2002 2:50 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.36 ug/1 755726 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 64 2 2,5-Dihydrophosphole, 3-methyl-l ... 192 C11H13OP 1000196-97-5 59 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 50 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 4768 (31.094 min): 08483.D (-4755) (-) m/z 192.10 100.00% 192
5000
40 82 96 146 160 30.80 31.00 31.20 31.40 miz-> a.52 . 70.„ . 118... a..I.. Hp 1 20 30 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 m/z 191.10 25.47% Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192
5000 30.80 31.00 31.20 31.40 175 m/z 96.10 17.09% — 63 89 145 45 | 77 10 117 z-> 20 30 40 50 60 70 80 90 100 110120130 140 150 160 170 180 190 200 135 II. 163 .. । I't1.. 11 .Trl'i... । .■!.. 11 i'I 11.... i1 lp Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl- 164 192 30.80 31.00 31.20 '31'46' 5000 99 m/z 193.10 14.84% 115 47 77 177 67 h ,‘ 1.57pr 87, 125,34 146 miz-> -7-=====**“ wl--+p4l++r+455. H 20 30 40 50 60 70 80 90 100 110 120130 140150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 192 30.80 31.00 31.20 31.40 m/z 146.10 14.22% 5000
27 39 96 a .!.... 51 p,.. (63r.,, [. ri. 82 39 .51 ( pl ।. rglij’t. ।176 139 i.152 126,.... 115 11111 |‘H "l’t rf ।. [■>■.•>. . 111. i i’„|| l’t .. ।. /z—> 20 30 40 50 60 70 80 90 100110120130 140150160 170180190 200 30.80 31.00 31.20 31.40
08483.D SCAN020418.M Thu May 02 11:45:00 2002 Page 6
NYC-WTC_000048644
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NYC-WTC_000048644Source: NYC Law Department, mirrored locally
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