GCMS quantitation results for sample AE10243, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10243.D Vial: 19 Acq On : 17 May 2002 3:08 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C: \MSDCHEM\1\METHODS\SCAN020507 .M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 4-Hydroxy-3,5-dimethylcinna ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.24 ug/1 18914 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 50 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 47 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 47 4 Phenanthrene, 1-methyl - 192 C15H12 000832-69-9 47 Abundance Scan 4768 (31.094 min): 10243.D (-4759) (-) m/z 192.05 100.00% 192

5000 146 ----- 96 30.80 31.00 31.20 31.40 ,1 441 I ' 701 11,11 1 ,1 - 442 ■ i m/z 191.10 29.98% m/z-> 50 100 150 200 250 300 350 400 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 30.80 31.00 31.20 31.40 63 89 145 m/z 146.10 27.94% 117 , 43, L uh Li. ul —frit r . 1 164 nz-> 50 100 150 200 250 300 350 400 Abundance #125842: Phenanthrene, 2-methyl- 192

30,80 31,00 31.20 31.40 5000 m/z 96.00 21.56%

96 , 39 63 .1 116 139 190 i । 4*fA"I ।■ । । i f i“i '•i •n/z-> 50 100 150 200 250 300 350 400 Abundance #81033: Phenanthrene, 9-methyl- ■ 1 i ■ ■ 192 30.80 31.00 31.20 31.40 m/ Z 83.90 18.03%

5000 J 96 165 39 63 .1 116 139 J, i [ i" 1*03T i" । ( i p i-1 n/z-> 50 100 150 200 250 300 350 400 30.80 31.00 31.20 31.40

10243.D SCAN020507.M Fri May 17 10:43:10 2002 Page 5

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