GCMS chromatographic data for sample AE10302, May 28, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10302.D Vial: 25 Acq On : 17 May 2002 9:03 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.30 ug/1 24315 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 50 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 4 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 42 Abundance Scan 4769 (31,100 min): 10302.D (-4757) (-) m/z 192.10 100.00% 19/2

5000 96 84 146 160 30.80 31.00 31.20 31.40 42 53 ' i " '11" " i " " i" " i - m... —136.1... 'I......... fl m/z 96.10 24.97% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 4

5000 1 30.80 31.00 31.20 31,40 m/z 146.20 19.38% 29 39 51 63 74 83 * 115 126 139 152 165 176 | | 1W—O——T—OUTTTTHmt 111" miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125844: Anthracene, 2-methyl- 1'12

30.80 31.00 31.20 31.40 5000 m/z 193.00 17.75%

93 96 165 “r, । , IIII'l , । . . . . । 115 63 74 11* 139 150 | 176 , i i i । i m । i i i C| , i i i | i i i > । ’Il i | I i I i । i i ‘rrrrrT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- 1 1 i ■ 1 ■ 1 i ' I ' ' ‘ ' I ' ' 192 30.80 31.00 31.20 31.40 m/z 160.10 15.12% 5000

96 27 39 51 63 82 . l 115 126 139 152 165 176 ' r "111'" i " " i'1 ■ ■ i' i TmmmpHput 11) 1 1 1 1 1 1 1 1 --- n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

10302.D SCAN020507.M Fri May 17 10:54:12 2002 Page 5

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