GCMS chromatographic data for sample AE10302, May 28, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10302.D Vial: 25 Acq On : 17 May 2002 9:03 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 15.46 0.23 ug/1 16835 Naphthalene-d8 16.53 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Cylopentasiloxane, decamethyl- 370 C10H3 0O5Si5 000541-02-6 53 3 PMenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 37 4 y-Methyladrenaline, tri-TMS_________413 Cl9H39N03Si3 1000071-72-1 37 Abundance Scan 2107 (15.459 min): 10302.D (-2098) (-) m/z 73.10 100.00% 73

5000 267 355 ■ ■ i ■ 1 ■ ■ i ■ ■ 45 15.20 15.40 15.60 15.80 i! i i 237 285 ---- ----- .................... .......... m/z 355.10 30.44% ■ । ‘ ■ ■ ।"" । 111" i ' i" " I'1 ‘' r 1 ’ I ’ ’’I’’ n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

5000 267 15.20 15.40 15.60 15.80 355 m/ z 2 67.00 30.13% 45 T 28 1 11——01’"1—000—000—2p009pm0m 96 115133 165,193 223 249 |__ 2293 TIPWPpuurrm 323 nz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 15.20 15.40 15.60 15.80 267 45.00 5000 m/ Z 13.49%

45 207 249 323 , [ ■| ‘ | | । | r Priyi ' 1 I ' ' ' ' 1 1 ‘ 1 ITTTi 1 1 'Pl | | i r | i > < ‘Tr 111 i i 11 ri 111 i i i| i । r 11 i *i 1111 i 11 । m/z-> 20 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73 15.20 15.40 15.60 15.80 m/z 356.20 12.30% 5000 355 44

‘i‘ TTH93 130147 193 220237 267 294 .... 1384 ti i “1। *11■1111 n/z—> 20 40 60 80 100 120140160 180 200 220 240 260 280 300 320 340 360 380 15.20 15.40 15.60 15.80

10302.D SCAN020507.M Fri May 17 10:54:12 2002 Page 4

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