GCMS re-analysis comments for sample AE10519, May 29, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\10519.D Vial: 9 Acq On : 21 May 2002 4:17 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 3 R.T. EstConc Area Relative to. ISTD R.T. 31.09 0.29 ug/1 32064 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene , 9-methyl- 192 C15H12 000883-20-5 64 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 3 Bitoscanate 192 C8H4N2S2 004044-65-9 53 4 Bitoscanate 192 C8H4N2S2 004044-65-9 53 Abundance Scan 4767 (31.088 min): 10519.D (-4759) (-) m/z 192.10 100.00% 192

5000

82 160 AM—A 47 374 439 30.80 31.00 31.20 31.40 III ill "l 0- — I t ,1) ,120J -r*J | — ' i ■ ■ ■ ■ i ' ■ ' 1 i ' ' i ' ' ' ' i m/z 191.20 28.35% n/z-> 50 100 150 :200 250 300 350 400 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 A 30.80 31.00 31.20 31.40 m/z 160.20 16.17% 96 165 । 0- 39 63, .1 115 139 4 m/z—> 50 100 150 200 250 300 350 400 Abundance #125847: Anthracene, 2-methyl- 192 ........ »I.... .... 30.80 31.00 31.20 31.40 5000 m/z 82.00 15.27%

28 63..9 115 139.165.............................. 0- ‘1 [ .■ । . t । ...if... r । । । । । i । । i । । । । n/z-> 50 100 150 200 250 300 350 400 Abundance #80930: Bitoscanate 192 30.80 31.00 31.20 31.40 m/z 84.10 13.77% 5000 134 90 160 AA 63 0 , । ‘ h 4 A A1.109 ., r , " 11 i 1 ................ /z—> 50 100 150 200 250 300 350 400 30.80 31.00 31.20 31.40

10519.D SCAN020521.M Fri May 24 09:20:34 2002 Page 5

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