GCMS re-analysis comments for sample AE10519, May 29, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\10519.D Vial: 9 Acq On : 21 May 2002 4:17 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Phenol, 6-methyl-2-[(4-morp... Concentration Rank 4 R.T. EstConc Area Relative to.ISTD R.T. 28.91 0.22 ug/1 24672 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phendl, 6-methyl-2-[(4-morpholin... 207 C12H17NO2 060460-71-1 5 2 6-Deoxyhemigossypol 244 C15H1603 055824-28-7 5 3 1,2-Okazino[2,3-b]isoquinolin- 10... 209 C12H19NO2 1000196-76-2 5 4 1,3,5 Triazine, 2-chloro-4,6-bis. . . 207 C5H6C1N3S2 004407-40-3 5 Abundance Scan 4396 (28.908 min): 10519.D (-4386) (-) m/z 207.10 100.00% 207

244 5000 67 86 51 172 38 109 136 — l). ITiT TII

n/z-> 0 I ' ‘ 20 ' I 40 60 80 1 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20 m/z 244.00 63.50% Abundance #84739: Phenol, 6-methyl-2-[(4-morpholinyl)methyl]- 207 u 86

5000 121 . ..... j.lj.... .... 28.60 28.80 29.00 29.20 57 m/ z 208.90 50.30% I 100 134 149160 176 0 41 .4 1 74 ■ 14—5 . ■#, । ■ 1 ■ • i v 199,44.11.. miz-> 20 40 60 80 100 120 140 160 180I 200 220 240 Abundance #92183:6-Deoxyhemigossypol 2-4

226 • • । > 28.60 28.80 29.00 29 20 5000 m/z 67.40 47.80%

115 128 183 198 211 139 155 .

m/z-> 0 20 40 60 80 97 in JO H , , M, I , sh , — — I—240 100 120 140 160 180 200 220 Abundance #35081:1,2-Oxazino[2,3-b]isoquinolin-10-one, perhydro 86 -.. III.,..I 28.60 28.80 29.00 29.20 m/z 210.90 46.97% 41 123 209 5000 67 27 99 136 151 II al 119, I ] ■ Il',/166.,,1921 166 180, - 0 IL, . iz-> 20 40 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20

10519.D SCAN020521.M Fri May 24 09:20:34 2002 Page 4

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