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GCMS analysis results for sample AE10243, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10243 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024824–000024831

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10243.D Vial: 21 Acq On : 10 May 2002 6:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 3-(2-Methoxy-5-methylphenyl... Concentration Rank 2

R.T. EstConc Area Relative to. ISTD R.T.

31.09 0.34 ug/1 46992 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 50 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 47 3 1,3 -Benzodioxole, 4-methoxy-6-(2 .. . 192 C11H12O3 000607-91-0 47 43,5-Ethanoquinolin-10-ol,decahy...209C13H23NO 021041-43-0 45 Abundance Scan 4767 (31.088 min): 10243.D (-4751) (-) m/z 192.10 100.00% 192

5000

A — 96 160 30.80 31.00 31.20 31.40 4370| 132 , 496 rT l[l N [ l| I h I lli | 1 "I.h 1 —I 11 1dT m/z 193.10 20.56% m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192 fl

5000 77 105 132 ...fl... 30.80 31.00 31,20 31.40 m/ z 160.20 17.81% 51 —lh ( 4.h,k 4,4 1 200 250 300 350 400 450 500 n/z-> 0 50 100 150 Abundance #80895:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- 192 ■ ■ i 1 ■ 1 ■ i ■ ‘ I....... ' I ‘ 1 1 ' I 1 1 30.80 31.00 31.20 31.40 5000 m/ z 96.00 15.76% 91 165 39 65 119 , , , 1,4 /4,4 1,4.4 200 250 300 350 400 450 500 mlz-> 0 50 100 150 Abundance #125822:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- ■ ■ i ■ । > j 192 30.80 31.00 31.20 31.40 m/ z 191.20 13.67%

5000 91 165 39 65

15,411, m/z—> 0 50 100 150 200 250 300 350 400 450 500 30.80 31.00 31.20 31.40

10243.D SCAN020507.M Tue May 14 14:25:54 2002 Page 4

NYC-WTC_000024829

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NYC-WTC_000024829Source: NYC Law Department, mirrored locally

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