GCMS analysis results for sample AE10243, May 2002

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Laboratory report documenting GCMS analysis of sample AE10243 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024824–000024831

Folder label: “GCMS X 5/14/02 A 5/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10243.D Vial: 21 Acq On : 10 May 2002 6:23 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to. ISTD R.T.

31.95 0.34 ug/1 46015 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

— 1 Anthracene-dlO- 188 C14D10 001719-06-8 80 2 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 40 3 Nickel, di-.mu.-carbonylbis(.eta... 302 C12H10Ni2O2 012170-92-2 38 4 Phenanthrene-diO________________ 188 C14D10 001517-22-2 37 Abundance Scan 4914 (31.951 min): 10243.D (-4907) (-) m/z 188.15 100.00% 188

5000

80 42 62 158102 132 31.60 31.80 32.00 32.20 - 352 11 f m/ Z 80.00 19.88% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79826: Anthracene-d10- 188

5000i 31.60 31.80 32.00 32.20 m/z 189.10 18.78% 94 160 I,

miz-> 1720 4042 6066.1114 .......... Ill... 111111111111Y111!11111"111111' i " 111 ■' 1P* ■' l " n 1111111 r‘111' u ' I ‘ " 11'''' I ‘1 ‘' I'''11 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 ............................. ...................... 31.60 31.80 32.00 32.20 5000 m/z 184.10 11.61% 143 64 89। . 115 170

miz-> - [ H " I " " I " " 11" 1 r " ' i " " i " " i " " r 1" i 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79885: Nickel, di-.mu.-carbonylbis(.eta.5-2,4-cyclopentad... 188 31.60 31.80 32.00 32.20 m/z 158.00 9.17% 246 5000 123

28 58 97 1’11 -+774 Th 141 "TT I60 ... h.. 21811 1 r ■ ■' i miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.60 31.80 32.00 32.20

10243 .D SCAN020507.M Tue May 14 14:25:55 2002 Page 5

NYC-WTC_000024830

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NYC-WTC_000024830Source: NYC Law Department, mirrored locally

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