GCMS analysis results for sample AE11154, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11154.D Vial: 19 Acq On : 22 May 2002 2:08 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.36 ug/1 37591 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

dPhenanthrene-di 0 188 C14D10 001517-22-2 68 2 Anthracene-dlO- 188 C14D10 001719-06-8 64 3 3-Amino-4 -methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 38 4 Nickel, di-.mu.-carbonylbis(.eta... 302 C12H10Ni2O2 012170-92-2 38 Abundance Scan 4914 (31.952 min): 11154. D (-4908) (-) m/z 188.15 100.00% 188

5000

80 94 160 41 55 . 118 224 312 31.60 31.80 32.00 32.20 0ttTTTT - - m/z 93.90 20.01% i - I ' ' 1 ' I * 1 1 'F ' 1 1 l 1 ' ' 1 I 1 ' 1 ' I mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 __ Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 80 94 m/z 94.30 19.64% 160

m/z-> 0-39 20 — 52 66 J „ll 108 132146 1 THTnTTTHT | ‘ ' 1 | i • • ' l ' «T* ] 1 1 ' 1 1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79826: Anthracene-d10- 188

31.60 31.80 32.00 32.20 5000 m/z 80.10 18.11%

„ 80 94 160 0—30,.52,66.441181321464 । I’ । । l“n ) I | I I I । । । I । । । । i r i । miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ... Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 31.60 31.80 32.00 32.20 m/z 189.20 16.06% 145 5000

117 159.'173

m/z—> 0Up +414441911,/ I i' 1 ■ i ■ ■ ■11 ■1 ■ ■ i11 ■ ■ i11'' i ■111111111 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 TtI --------------------- 31.60 31.80 32.00 32.20

11154.D SCAN020521.M Fri May 24 09:23:30 2002 Page 9

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