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GCMS chain of custody form, sample AE10240, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10240 on May 20, 2002, including surrogate compound data.

NYC-WTC_000024390–000024401

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024400
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10240.D Vial: 18 Acq On : 10 May 2002 3:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.38 ug/1 56133 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual **P l Phenanthrene-d10 188 C14D10 001517-22-2 64 —2 Anthrcene-d10- 188 C14D10 001719-06-8 45 3 1,2-Bis(2-hydroxyphenyl)ethylene ... 376 C24H28N2O2 1000187-13-2 38 4 1,4-Naphthalenedione , 2-hydroxy-.. . 188 C11H8O3 000483-55-6 32 Abundance Scan 4916 (31.964 min): 10240.D (-4905) (-) m/z 188.15 100.00% 188

5000 94 160 Ifm*I4IIIIIIIIIII 44 66 132 269 31.60 31.80 32.00 32.20 T-rp- " i'''11" " i ‘1" i " " I ’" 1 r 1" r ■ ‘' i " " i" ‘1 r ' m/ z 94.15 26.74% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 m/z 80.00 22.27% 80 160 |

m/z-> -3052 14 . 4..4.7 1' r " ■ i11" i " " i1 ‘■ i" " i " " i " " i" " r 1 20 40 60 80 100120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79826: Anthracene-d1 0- 188

31.60 31.80 32.00 32.20 5000 m/z 184.10 19.62%

94 17 42 66 4114132 160 ,h z-> 4.4.. *1111111 r* *11 r11 ■ ■1' r ■" i" " i " " i1"11'1" i" ‘' i " " i''1' i" 20 40 60 80 100120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79831:1,2-Bis(2-hydroxyphenyl)ethylenediamine, N,N'-bis(... 188 31.60 31.80 32.00 32.20 m/z 189.20 19.60%

5000

41 77 94 । 121 145 171 m/z— > -H 210 238255 “0— 293 377 20 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 31.60 31.80 32.00 32.20

10240.D SCAN020507.M Tue May 14 14:25:27 2002 Page 7

NYC-WTC_000024400

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NYC-WTC_000024400Source: NYC Law Department, mirrored locally

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