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GCMS chain of custody form, sample AE10237, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10237 on May 20, 2002, including surrogate compound data.

NYC-WTC_000024380–000024389

Folder label: “GCMS X 5/1/02 A 5/9/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020509\10237.D Vial: 15 Acq On : 10 May 2002 12:27 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 *********************************************************** * ********* Peak Number 3 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.34 ug/1 42734 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Phenant ene-d10 188 C14D10 001517-22-2 59 2 2-Quino inecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 38 3 1,4-Nap thalenedione, 5 - hydroxy-.. . 188 C11H8O3 000481-42-5 37 4 2,2,9/9 Tetramethyldec-5-ene-3,7...188C14H20 102745-35-7 32 Abundance 7 Scan 4914 (31.952 min): 10237.D (-4905) (-) m/z 188.20 100.00% 1(8

5000 80 94 31.60 31.80 32.00 32.20

m/z-> +++4149. ++. i-q-r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.30 26.81% Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 m/Z 80.00 23.08% 80 94 160 30 42 52 66 । 102110118 132 146 nJ 170180 \ | I i 1 I | 1TT7 t 1 1 1 । I I 1 1 | 1 I ri 1 H-| H 1 I | I I 1 1 | » 1 11 । i ri 1 । 1 1 1 । । | 1 1 1 । 1 । 1 । । t 1tP|'i 1 1 1 1 1 1 1 1 I PPlT] 1 1 1 1 ।

n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance■ #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188

31.60 31.80 32.00 32.20 5000 m/z 184.10 16.56% 143 . 89 115 158 170 n/z-> 51 ■ i... ................... 111' । |'i 11 4,76,4102 . -HH .mmH 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Tnun 130

Abundance #125695:1,4-Naphthalenedione, 5-hydroxy-2-methyl- 1(18 31.60 31.80 32.00 32.20 m/z 189.20 11.69% 5000 63 92 131 120 51 160 173 103 145 — ' i"1111" |_i"11 lllini "m - Wn ,11317 TTT m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31,60 31.80 32.00 32.20

102’7 n cfAwnoncm M M- , 1 A 1 A

NYC-WTC_000024388

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NYC-WTC_000024388Source: NYC Law Department, mirrored locally

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