GCMS analysis results for sample AE08486, May 2002

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Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048647–000048659

Folder label: “GCMS X 4/10/02 A 4/20/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08484.D Vial: 21 Acq On : 20 Apr 2002 3:49 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.40 ug/1 930552 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 59 2 Anthracene-dlO- 188 C14D10 001719-06-8 47 3 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 40 4 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 38 Abundance Scan 4915 (31.957 min): 08484.D (-4902) (-) m/z 188.15 100.00% 118

5000 40 80 94 "it ----- 31.60 31.80 32.00 32.20 'ri ■ । itTi i 111 > n-t THm 49 ©6 .. ij. m/z 40.10 20.16% miz-> 10 20304050607080 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 " ' ' 80 94 160 m/z 94.10 17.33% ......... aun6 30 66 42 52.... 1108118 132 146 170179,III___ I.. < I! >... I. ■.. 11,.. I H 1111111 prh 1111 [ 1111111111 > 11111! 11 fl 11! 1111! 11 rl’l 11111111 r’l’l nu rnfe-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d1 0- 118

31.60 31.80 32.00 32.20 5000 m/z 189.20 16.26%

80 94 eeVwY* 160 I. 17 30 42 52 P . j 108118 132 146 1 170179,1 r Aampoazayorottass—tavytlagaad/8am fti 111 ,T|,,, 11 >,.. 11, ।,, n 1. 111 "l‘ i i n 111., MI’l’ ) in. miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 1(8 31.60 31.80 32.00 32.20 m/z 80.10 13.03% 5000

143 89 115 51 64 76 I 102 || 130 1, 158 170 । iz—> TH TTWTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTH - ruilmnaspaaapla TTTr 10 20 30 40 a) 60 70 80 90 100110120130140150160170180190 -------------------- 31,60 31.80 32.00 32.20

08484.D SCAN020418.M Thu May 02 11:45:27 2002 Page 7

NYC-WTC_000048657

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