GCMS analysis results for sample AE08486, May 2002

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Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048647–000048659

Folder label: “GCMS X 4/10/02 A 4/20/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08484.D Vial: 21 Acq On : 20 Apr 2002 3:49 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 6-Nitro-2-methylpyrrolo [2,3... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 40.44 0.20 ug/1 434653 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6-Nitro-2-methylpyrrolo[2,3-g]qu... 227 C12H9N3O2 1000071-35-1 47 2 5-Cyano-8-dimethylamino-6-methox... 227 C13H13N3O 1000213-20-5 33 3 5-Cyano-2-methyl-6-phenyl-4-thio... 227 C12H9N3S 013996-07-1 28 4 2-Fluoro-4-methyl-10H-acridin-9-one 227 C14H10FNO 1000210-25-9 23 Abundance Scan 6358 (40.436 min): 08484. D (-6351) (-) m/z 227.20 100.00% 2.7

5000 40 57 dBBum 84 99 — P , a—44. 113 170 198 , 11 .240, 1 ‘ I ■ ■ L 40.20 40.40 40.60 40.80 m/z 113.60 25.67% I ‘ ' I • ‘ 1 • I ' • ' ‘ I ■ • ' ' I ‘ ' iz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #89088:6-Nitro-2-methylpyrrolo[2,3-glquinoline 2.7

......... ................................ 5000 181 43 40.20 40.40 40.60 40.80 57 m/z . 40.10 24.81%

nz-> ■ ’ I 40 15283 100 120 140 154169 I ' 11 1 r1 1 ' 60 80 97 160 180 200 220 4 197 240 Abundance #89117:5-Cyano-8-dirnethylarnino-6-methoxyquinoline 2.7 212 40.20 40.40 40.60 40.80 5000 rn/z 226.20 14.38%

1.98 42,52 63 76 88 101 114 127 141 155 169 184 l 1 i * । I 1 l • । '• i « I ‘ । t "i" i i |' i > r 1 1 1 PT—1—1 IMi—i—। 1 i—i—1" i r 1 I 11 1 1 1 ' 1 iz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #89096:5-Cyano-2-methyl-6-phenyl-4-thioxo-3,4-dihydropyri... . ................................ . 227 40.20 40.40 40.60 40.80 186 m/z 228.10 14.06%

5000

miz—> ......... ........................ ......... I... 40 60 80 100 120 140 160 180 200 220 ‘ 240 ‘ 153 1.....N..... 40.20 40.40 40.60 40.80

08484.D SCAN020418.M Thu May 02 11:45:28 2002 Page 8

NYC-WTC_000048658

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GCMS sample analysis report AE08483, May 7 2002 · Box DEP Box 27

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