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GCMS analysis results for sample AE08426, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048169–000048181

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08426.D Vial: 13 Acq On : 19 Apr 2002 7:57 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 2-Fluoro-4-methyl -lOH-acrid... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 40.44 0.20 ug/1 400267 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Fluoro-4-methyl -lOH-acridin-9-one 227 C14H10FNO 1000210-25-9 25 2 Aminobenzene, 2-hydroxymethyl-N-... 227 C14H13NO2 1000128-77-9 9 3 6-Nitro-2-methylpyrrolo [2,3-g]qu... 227 C12H9N3O2 1000071-35-1 9 4 2-Methyl-9-chloro-acridine 227 C14H10C1N 1000147-94-7 9 Abundance Scan 6358 (40.436 min): 08426.D (-6354) (-) m/z 227.20 100.00% 227

40 5000 113 A------ m/z-> 51 1. । . I' I r',’ , । , 40 60 85 98 ' ■ ''i hida J. r ■ ■ 80 100 120 ...... 170..794.... —IP 140 160 180 200 220 240 240 m/z 40.10 40.20 40.40 40.60 40.80 59.11% NAA—AARWWRRyA

Abundance #89104: 2-Fluoro-4-methy 1-1 OH-acridin-9-one Z!7

5000 198 40.20 40.40 40.60 40.80 m/z 113.50 24.90% , , , 13,,57,6777.89.92 113 125,140151, 179 1——n—nd—m—m——nTrTTTT+—+ 1 Hrio ,.| 208 ''I1>'|!> 184 /z—> 40 60 80 100 120 140 160 180 200 220 240 Abundance #89110: Aminobenzene, 2-hydroxymethyl-N-[2-hydroxybenzylid... Z7 ........................ ............................... 106 180 209

77 40.20 40.40 40.60 40.80 5000 93 m/Z 228.10 23.07% 51 65 121 | 132,152 167 196 LUA + 1-/.142.l- all., . . — 1 1 i ‘ ■ /z-> Abundance 40 60 80 100 120 140 160 180 #89088: 6-Nitro-2-methylpyrrolo[2,3-g]quinoline 200 220

2.7 240 A 40.20 40.40 40.60 40.80 m/ z 226.10 18.29%

5000 181 43 57 I, 69 93 154 | 169 197 . , Il , II I , 83 97 . . Tikn r ■ > I T r ■ < | i I I r I I I t 1" n/z-> 40 60 80 100 120 140 160 180 200 220 240 40.20 40.40 40.60 40.80

08426.D SCAN020418.M Thu May 02 15:30:24 2002 Page 8

NYC-WTC_000048180

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NYC-WTC_000048180Source: NYC Law Department, mirrored locally

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