GCMS analysis results, Sample AE08264, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08264.D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 para-Methoxybenzenethiol Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

13.63 0.23 ug/L 367672 Napthalene-d8 13.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 para-Methoxybenzenethiol 140 C7H8OS 000696-63-9 64 2 2,5-Cyclohexadiene-1,4-dione, 2,. 140 C6H404 000615-94-1 39 3 2-Hydroxy-5-nitropyridine 140 C5H4N2O3 005418-51-9 38 4 5-Fluoronicotin amide 140 C6H5FN20 1000126-56-3 38 Abundance Scan 1796 (13 632 min) 08264.D (-1785) (-) m/z 140.00 100.00% 140

5000

.................. PP—n । ■ ■ ■ 94 , 64. 70 13 40 13 60 13 80 14 00

n/Z—> 0— 10 20 30 42 52 I#, I .-i ll........I , . 40 50 60 70 80 22444444 90 112 —r > > > i * > 1 i ■ ■ •' i ■ ’ 100 110 120 130 140 150 m/z 70.00 13.59% Abundance #63646: para-Methoxybenzenethiol 140 125

5000- 97 13.40 A 13.60 . 13.80 14 00 m/z 141.10 12.73% , 22 69 /z- > 01 . . . I— —15.27—88.7.74.2+17784.ll, - 10 20 30 40 50 60 70 80 90 100 109 110 120 130 140 150 Abundance #122847: 2,5-Cyclohexadiene-1.4-dione, 2,5-dihydroxy- 14.0 ‘IS’’’ j ‘ . r . /‘‘ 13.40 13.60 13.80 14 00 42 5000 m/ Z 94.00 12.21% 69

53 84

0- ....... 3.29,l 1L. 8 77 94 103 112119 126 133 - — Tl/Z-> 10 20 30 40 50 60 70 90 100 110 120 130 140 150 Abundance #63571 2-Hydroxy-5-nitropyridine 14 0 13.40 13.60 13.80 14.00 m/z 66.00 8.71% A 5000 66

80 93 110 124 131 0 ..... . ,44 „l. | 4 trrit .1.103,111 TITTT I tVz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 13.40 13.60 13.80 14.00

08264.D 041702SCAN.M Thu Apr 18 09:52:45 2002 Page 15

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