GCMS scan report for Method 508, April 2002

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Data File : C:\MSDCHEM\1\DATA\020419\08485.D Vial: 22 Acq On : 20 Apr 2002 4:48 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Pyrimidinetetramine - Concentration Rank. 14

R.T. EstConc Area Relative to ISTD R.T.

16.76 0.24 ug/1 457752 Naphthalene-d8 16.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- 140 C4H8N6 001004-74-6 59 2 2-Hydroxy-5-nitropyridine 140 C5H4N2O3 005418-51-9 50 3 para-Methoxybenzenethiol 140 C7H8OS 000696-63-9 45 4 Pyrimidine, 2,5-dimethoxy- 140 C6H8N2O2 016290-94-1 42 Abundance Scan 2329 (16.763 min): 08485.D (-2321) (-) m/z 140.10 100.00% 140 A 40 5000 ................................................

70 94 16.40 16.60 16.80 17.00

miz-> 0- ' ' I' ■ ■ ‘ I ''' ‘ I ‘' 1' ' T-l-p- 60 78 86 If 108 — , J 111. IH# - - ‘ ! I I ■>- >!' 11 -1 - - 10 20 30 40 50 60 70 80 90 100 110 120 130 140 I m/ z 40.10 51.82% Abundance #63524: Pyrimidinetetramine- 140

5000 43 16.40 16.60 16.80 17.00 71 123 m/z 70.10 16.75% 28 ,il — 86 96 112

mz-> 01 10 20 l —4l++ 1—79++44105-1 30 40 50 55 60 70 80 TTTTITT 90 100 110 120 130 140 ‘IT

Abundance #63571:2-Hydroxy-5-nitropyridine 1-0

16.40 16.60 16.80 17.00 5000 m/z 141.00 12.85% 66

80 93 110 55 44 0-mmPTTTT TTTH -44L+741l +4 ......... 124 131 TTTTLTTr I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63646: para-Methoxybenzenethiol 1-0 16.40 16.60 16.80 17.00 125 m/ z ,94.10 12.44%

5000 97 69

mfz-> 0 —15.27,31.72 ,60^1,470.77.84 10 20 30 40 50 .,. 1-1 mpg |l" ।... 1. 80 90 100 110 120 130 140 109 ------------ 16.40 16.60 16.80 17.00

08485.D SCAN020418.M Mon Apr 29 08:30:59 2002 Page 14

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