GCMS scan report for Method 508, April 2002

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Data File : C:\MSDCHEM\1\DATA\020419\08485.D Vial: 22 Acq On : 20 Apr 2002 4:48 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 2,4-Diamino-6- (hydroxymethy . . . Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.40 ug/1 852027 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4-Diamino-6-(hydroxymethyl)pte. .. 192 C7H8N6O 000945-24-4 64 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 50 73 Anthracene, 9-methyl- 192 C15H12 000779-02-2 50 4 Anthracene, 9-methyl-_______________ 192 C15H12 000779-02-2 50 Abundance Scan 4767 (31.088 min): 08485.D (-4759) (-) m/z 192.10 100.00% 152

5000

40 49 70 92 । 96 J 118 146 160 | ... y . 30.80 31.00 31.20 31.40 0-PTTTTHHPmmmTLTTT i'."T " H1 TT m/z 191.00 19.52% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125821:2,4-Diamino-6-(hydroxymethyl)pteridine 43 192 163

5000 28 30.80 31.00 31.20 31.40 53 68 146 175 m/z 96.00 14.67% 121

m/z-> 0 — 4X-HHlll ‘ITT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 92 106 133

Abundance #125842: Phenanthrene, 2-methyl- 1912

30.80 31.00 31.20 31.40 5000 m/z 146.10 13.56%

96 82 THHrTj I I1l i [ i H l I 115 126 139 152 165 176 . 27 39 51 63 0 Fit i J > > I I | I I 11 l'| I | ri 1*1 I | I | i’t’i 1 | | I’I'I T 1‘l‘ Wrrr m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- 192 30.80 31.00 31.20 31.40 m/z 160.10 11.66% 5000

96 165

ti/z-> 0 i l । 28 39 51 63 74 83 I 105 115 126 139 152 1 176 , ■ f/1 । । 10 ii । |'i | । । । ITi || j I’fi i'I'i I'l'j il I l| : | i : | r’i i । i i I I । । । । i'j | | J J |'l 1 | I [ 1 + tl | J rli | 1 1 ! I

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 —... 0...... 30.80 31.00 31.20 31.40

08485.D SCAN020418.M Mon Apr 29 08:31:01 2002 Page 15

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