GCMS scan report for Method 508, April 2002

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Data File : C: \MSDCHEM\1\DATA\020419\08485.D Vial: 22 Acq On : 20 Apr 2002 4:48 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ************************************************ * * ******************* Peak Number 3 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.42 ug/1 889228 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 hracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 86 3 7-Tetradecene-5,9-diyne, (E)- 188 C14H20 013304-98-8 42 4 Phosphonic acid, (3-methyl-3-pen. . . 188 C8H13O3P 022152-34-7 38 Abundance Scan 4915 (31.957 min): 08485.D (-4904) (-) m/z 188.15 100.00% 188

5000

80 94 .......................... ................. , , , , , 66 160 31.60 31.80 32.00 32.20 0 mpmmmmmmmMmTH ntt 1’1100111111711111311118011110103-" ’ITT Tmn m/ z 80.20 21.13% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 1ST । ■ ■ ■ ■' । > 1 i ■ । i i 1 1 I 1 31.60 31.80 32.00 32.20 m/z 189.20 18.62% 66 80 94 160 , , 17 30 42 52 108118 132 146 11. 170179,| 0 TLWWTTTTTTTNNT 11' 111111111'11' 11111 [ 11 ■ 1111.111111111111 > trmri Hmn 1111111 “’t ।,, ‘I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 US T-r-F i ■ • ' 1 i ■ ■ ■ ■ i ' ' ■ ■ i ' 31.60 31.80 32.00 32.20 5000 m/z 94.05 18.01%

80 94 160

m/z-> 30 42 52 66 l| 108118 132 01IIWWmtphtt rj 1111111 n। n 11111111111» 148.-4,179179 — 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79740:7-Tetradecene-5,9-diyne, (E)- 1(8 31.60 31.80 32.00 32.20 91 117 131 rn/z 184.10 13.65% 5000 41 77 103 145 51 I 159 II I ............... ,,,,,, 0 < i ■ ■ i ■"1 i'"' i" " i • * * ■ i ■ ‘ • i1" 1 ‘ i" " i • ’ 1’1 I “"I m/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

08485.D SCAN020418.M Mon Apr 29 08:31:03 2002 Page 16

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