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GCMS analysis results for sample AE11305, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11305 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024613–000024622

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020516\11305.D Vial: 16 Acq On : 17 May 2002 12:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.28 ug/1 20705 Phenanthrene-dl0 31.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 74 2 Phenanthrene-diO 188 C14D10 001517-22-2 68 3 Pentacyclo[7.3.1.1. (4,12) .0(2,7) ... 188 C14H20 1000215-61-8 47 4 Phosphonic acid, (3-methyl-3-pen... 188 C8H13O3P 022152-34-7 43 Abundance Scan 4914 (31.952 min): 11305.D (-4907) (-) m/z 188.20 100.00% 188

5000 94 44 52 66 80 31.60 31.80 32.00 32.20

mlz-> -HmmmHT ■ i'"11" " i ■ 160 I I 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 m/ z .94.10 23.54% Abundance #79826: Anthracene-d 10- 188

5000 31.60 31.80 32.00 32.20 m/z 184.30 19.77% 80 94 160 17 30 42 52 66 108 118 132 146 1 170179/1 TT 1 " I " 1111 " ' 11 rri 1111 jil.... It "I"" ................IIapulanaapummt Wr n/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1(18

31,60 31.80 32.00 32.20 5000 m/z 189.15 18.69%

80 94 160 30 42 52 66 , 11 108 118 132 146 I,170179, 111 ।।11111111ITT 11. । j I. 1111.. +tt1 1*1111111111111111111111111111111111 i'ItPi iiii miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 1(18 31.60 31.80 32.00 32.20 m/ z 80.10 18.15% 5000 79 91 55 67 105 131 105 117 /z—> ' I " " 11'" I' ‘‘ 1'' । 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 145 159 173 L I 31.60 31.80 32.00 32.20

11305.D SCAN020507.M Fri May 17 13:12:50 2002 Page 5

NYC-WTC_000024621

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NYC-WTC_000024621Source: NYC Law Department, mirrored locally

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