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GCMS analysis results for sample AE11305, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11305 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024613–000024622

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024620
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\11305.D Vial: 16 Acq On : 17 May 2002 12:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 1,5-Naphthalenedithiole Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.10 0.24 ug/1 17685 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 53 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 52 3 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 52 4 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 52 Abundance Scan 4769 (31,100 min): 11305.D (-4759) (-) m/z 192.10 100.00% 192

5000

on 146 30.80 31.00 31.20 31.40

z-> TI*mumHu 51 70 .,19.. ....................... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.20 30.44% Abundance #80950:1,5-Naphthalenedithiole 192

5000 159 30.80 31.00 31.20 31.40 115 128 m/z 146.20 23.00% 40 57 69 79 96 147 I | ■ I ■ I | l~> t l'1'l'l1! I |'l n | Ir fpeereptrerrp, r l rlp I 177 T11111 1 niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- 19 2

30,80 31,00 31.20 31.40 5000 m/z 193.30 16.28%

96 27 39 51 63 J82 115 126 139 152 165 176 ■ i ■ ■" i " " r " ■ i "'111 TTpr’i ■ 11' ।■1 riri 111"111 ITr 1111 pi 1111 i’r 111 rI 11111!1 Tp-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81041: Phenanthrene, 3-methyl- 192 30.80 31.00 31,20 31.40 m/z 81.80 16.02% 5000

27 39 51 63 82 96 j| 115 126 139 152 190 176 P 11 “ " r ‘ " r 1" 1" " I" p >' > fl । rh '111 r'11 ITTn । p 11111111'11111 pi 1111 i’i'i । TTHT i-p-r n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31,00 31.20 31,40

11305.D SCAN020507.M Fri May 17 13:12:50 2002 Page 4

NYC-WTC_000024620

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NYC-WTC_000024620Source: NYC Law Department, mirrored locally

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