GCMS sample AE11154 analysis with surrogate recovery, May 2002

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Data File : C:\MSDCHEM\1\DATA\020515\11154.D Vial: 20 Acq On : 16 May 2002 6:34 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 1,5-Naphthalenedithiole Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.34 ug/1 34884 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 53 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H130P 1000196-97-5 53 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 50 4 Benzene, 1-bromo-2-chloro- 190 C6H4BrCl 000694-80-4 47 Abundance ‘ Scan 4768 (31.094 min): 11154. D (-4755) (-) m/z 192.10 100.00% 192

+ 5000

. 76 146 42 „ | 1120 393 543 30.80 31.00 31.20 31.40 n- -HA- m/z 191.10 22.71% n/z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #80950:1,5-Naphthalenedithiole 192

5000 U 30.80 31.00 31.20 31.40 128 159 m/z 194.10 17.81% 40 79 iT , -4,4— .4..*..... .............. . .................. ...... . m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl- 164192 .. Il .. 30,80 31,00 31.20 31.40 5000 99 m/ z 76.10 14.19% 47

mlz-> 0 L —+ 50 4112, 100 25

150 200 250 300 350 400 450 500 550 Abundance #80862:1,2-Phenylene diisothiocyanate ‘ * I 1 1 1 1 I * ' ’ * I 1 1 i ■ ■ 192 30.80 31,00 31.20 31.40 m/z 146.10 12.92% 64 5000

90 134 39 4 | 160 .1 1i l + |i A. J I I ,---PPI- n/z—> 0 50 100 150 200 250 300 350 400 450 500 550 30.80 31.00 31.20 31.40

11154.D SCAN020507.M Thu May 16 14:37:46 2002 Page 6

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