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GCMS results for sample AE11425, May 29, 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS analysis for sample AE11425 conducted on May 29, 2002.

NYC-WTC_000022526–000022538

Folder label: “GCMS X 5/17/12 A 5/21/02

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Scanned page image, NYC-WTC_000022536
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11425.D Vial: 11 Acq On : 21 May 2002 6 :15 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 1,5-Naphthalenedithiole Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.10 0.30 ug/1 32641 Phenant hrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5 -Naphthalenedithiole 192 C10H8S2 1000223-69-5 42 2 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 36 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 33 4 Bitoscanate Abundance V ______ ____________ 192 C8H4N2S2 Scan 4769 (31.100 min): 11425.D (-4758) (-) 004044-65-9 9 m/z 192.10 100.00% 192

5000

on 96 146 160 1 1 i ■ ' 1 ■ । TPmu 44 70 30.80 31.00 31.20 31.40

m/z-> 0 --- mm— —H ....... . " I — '1 82 । 120 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 | m/z 191.20 25.09% Abundance #80950:1,5-Naphthalenedithiole 192 JY 5000 ■ ■ i • ■ ■ 1 i ■ 44. 30.80 31.00 31.20 31.40 115 128 159 m/z 193.20 20.67% 40 57 69 79 96 147 177 0 11111 p । imp n’r । lrrrrpT’rrtpari rl’r 11 ill, p 11 pits I. ■'1 h11 TTTTTTT 1 • i ■ ■ n/z-> 20 30 40 50 60 70 80 90 1CX) 110 120 130 140 150 160 170 180 190 200 Abundance #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 192 .................. ' 1 I ' ' 1 ' 1 1 ' ■ i ' ' ■ ' i ■ ■ 147 30.80 31.00 31.20 31.40 5000 m/z 146.20 13.89% 45 । go 69 96 115

mz-> 27 J.44Hr.......... 134.. 0 TTT 1 rrpr rl 11 82 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 158 177 i“ Trp-r

Abundance #125842: Phenanthrene, 2-methyl- 192 30.80 31.00 31.20 31.40 m/z 160.10 12.98% 5000

96 27 39 51 63 82 . 1l 115 126 139 152 165 176 0 1200012W00m—02—311—————Tm7 1*111' I" ■ ।' ■'' । ■ ri111111 j 1111‘| > > 11 |‘l 111 (i'ri 111 " 111" ITII 1 1 i ■ ■ 1 ■ i ' ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

11425.D SCAN020521.M Fri May 24 09:26:47 2002 Page 7

NYC-WTC_000022536

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NYC-WTC_000022536Source: NYC Law Department, mirrored locally

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