GCMS analysis results for sample AE08429, May 2002

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Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048207–000048219

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\l\DATA\020419\08429.D Vial: 16 Acq On : 19 Apr 2002 10:54 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 1,5-Naphthalenedithiole Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.30 ug/1 630738 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 42 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 4 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 38 Abundance Scan 4767 (31.088 min): 08429.D (-4756) (-) m/z 192.10 100.00% 192

5000

96 40

m/z-> 1 " I " " i111 r'i 55 66 I " 11111 82 —H—H Tn118 , 146 160 rT ......................................... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l— m/z 30.80 31.00 31.20 31.40 96.10 18.82% Abundance #80950:1,5-Naphthalenedithiole 192

5000 ........... MIA 30.80 31.00 31.20 31.40 115 128 159 m/z 191.10 17.72% 147

/z-> .. ,40111157,.,163..7$47,.3,196,l.p1 +136—4 ........... . ........... ‘ I’’ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

30.80 31.00 31.20 31.40 5000 m/z 193.10 13.51%

45 69 82 90 .no । 122 134 1 148 160 ■ -Pmmmmmmmmmmmmmmmmmmmmmmm- '1111 n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 1 ' i 1 ' 192 30.80 31.00 31.20 31.40 161 m/z 146.20 13.25%

5000 77

/z—> mmmTT 52 64 91 103 MllH 138.77 ‘ I ‘ ‘II’’" "U 121 1 ■ I' ' 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 149

L 177

‘ 1 11 ........ 1 । I 1 1 1 1 I ' 1 30.80 31.00 31.20 31.40

08429.D SCAN020418.M Thu May 02 15:38:04 2002 Page 6

NYC-WTC_000048216

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GCMS analysis results for sample AE08431, May 2002 · Box DEP Box 27

NYC-WTC_000048121

Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.

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