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GCMS quantitation results for sample AE10246, May 2002

Machine-extracted title · confidence 90%

Laboratory report of GCMS analysis for sample AE10246 conducted on May 28, 2002.

NYC-WTC_000024871–000024882

Folder label: “GCMS X 5/14/02 A 5/17/02

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Scanned page image, NYC-WTC_000024880
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020516\10246.D Vial: 22 Acq On : 17 May 2002 6:05 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 1,5-Naphthalenedithiole Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.29 ug/1 21153 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5 -Naphthalenedithiole 192 C10H8S2 1000223-69-5 53 2 Thiophene/ 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 50 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40 Abundance Scan 4767 (31.088 min): 10246.D (-4755) (-) m/z 192.10 100.00% 192 Ik 5000

82 146 159 38 52 1 94 118 30.80 31.00 31.20 31.40

mfe-> H ' I “' 11 ' I' 111111" 11 P 11111" ' 111111"

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 193.10 25.02% Abundance #80950: 1,5-Naphthalenedithiole 192

5000 ' ' i ' ' ■ ■ i ' ' ■ i ■ ■ • ■ i ■ ■

159 30.80 31.00 31.20 31.40 115 128 m/z 191.00 24.03% 40 57 69 79 96 147 1111111 ri । h । r l । Ir |l|'i'i'i'J,-i'i-i-i'| ll, rI 111 l r 11 'i1 r" 11 A 111 —— 177 -rrp-r 'i " " r ■ mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81023: Thiophene, 2-[2-(3-thienyl)ethenyl- 1 2 .................................................

147 30.80 31.00 31.20 31.40 5000 m/ z 82.00 19.40% 45 c 69, 96 115

^z-> 27 ■ I"I' 44 -H41,195.1.7.. 14—lR 177 82 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 158 ■। i ■ ■ kp Abundance #125847: Anthracene, 2-methyl- 1 ' i 1 ■ ■ ■ i 1 1 ' I ' ' 1912 30.80 31.00 31.20 31.40 m/z 146.10 17.66%

5000

m/z-> 28 39 51 63 82 96 115 126 139 152 165 176 i । । > d । i i i l*j 1 I I I |'l I 1 1 | ITin । 1'1 i ।' Pi "’ll I 11'! | I I | ) TTrmi l t I | J J ! l’| | | | rth | J | t'l I I | I rl | J l ‘ f'l 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4-rrp-r ... n.... 30.80 31.00 31.20 31.40

10246.D SCAN020507.M Fri May 17 10:48:21 2002 Page 6

NYC-WTC_000024880

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NYC-WTC_000024880Source: NYC Law Department, mirrored locally

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