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GCMS Analysis Results, Sample AE08261, April 22, 2002

Machine-extracted title · confidence 100%

Initial analysis page for sample AE08261 showing surrogate recovery data and unknown compound screening.

NYC-WTC_000048287–000048308

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048302
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08261.D Vial : 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 1,5-Naphthalenedithiole Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.33 ug/L 615295 Phenanthranene- dl 0 23.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 40 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 4 Bitoscanate 192 C8H4N2S2 004044-65-9 38 Abundance Scan 3330 (22 645 min) 08261.D (-3323) (-) m/z 192.10 100.00% 15 2

5000

66 82 96 | 146 160 ' ' I ' ' ‘TI 22.40 22.60 22 80 23.00 4 42 52 01TPP** PHu 120 mmmmm—per m/z 191.10 21.98% Tl/Z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950: 1,5-Naphthalenedithiole 192

5000- 22 40 22 60 22.80 23.00 115 128 159 m/z 146.10 15.24% 69 79 — 96 147 57 n/z-> 01 -1 । 87 || 106 ,| 177 1TU01r +136, 41, " i ■ ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192 ................... /... 2240 22 60 22.80 23 00 5000 m/z 96.00 14.97%

45 | T 82 90 108 122 134 148 160 .. ....I------------- 1 o ■ i" " i ’ i" " i "‘‘T n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848 Anthracene, 9-methyl- 102 22 40 22 60 22 80 23.00 m/z 193.10 12.94%

5000

96 115 126 139 152 165 176 /Z—> 0-T 27 39 20 30 40 50 60 70 80 51 63 74 82 X 4 1 ■ i ■1 ‘*‘*111'1' i1 ’ ‘ ■... | i... । > ri. ।.. i. । 90 100 110 120 130 140 150 160 170 180 190 200 ■ ' I ' ' ’ ' I TT 22.40 22 60 22 80 23.00

08261.D 041702SCAN.M Thu Apr 18 09:47:23 2002 Page 12

NYC-WTC_000048302

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NYC-WTC_000048302Source: NYC Law Department, mirrored locally

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